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Bruker SMART APEXII CCD diffractometer4744 independent reflections
Radiation source: fine-focus sealed tube3744 reflections with I > 2σ(I)
graphiteRint = 0.027
[var phi] and ω scansθmax = 32.3°, θmin = 2.6°
Absorption correction: multi-scan (SADABS; Bruker, 2009)h = −16→15
Tmin = 0.950, Tmax = 0.992k = −17→17
17061 measured reflectionsl = −14→17