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Bruker APEXII CCD diffractometer4809 independent reflections
Radiation source: fine-focus sealed tube4141 reflections with I > 2σ(I)
graphiteRint = 0.026
ω scansθmax = 31.3°, θmin = 1.9°
Absorption correction: multi-scan (APEX2; Bruker, 2008)h = −8→8
Tmin = 0.803, Tmax = 0.917k = −18→18
18906 measured reflectionsl = −28→28