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Bruker SMART APEX CCD area-detector diffractometer4044 independent reflections
Radiation source: fine-focus sealed tube3433 reflections with I > 2σ(I)
graphiteRint = 0.028
[var phi] and ω scansθmax = 25°, θmin = 2.2°
Absorption correction: multi-scan (SADABS; Bruker, 2000)h = −10→10
Tmin = 0.626, Tmax = 0.645k = −12→12
8415 measured reflectionsl = −17→17