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Rigaku SCXmini diffractometer2969 independent reflections
Radiation source: fine-focus sealed tube2241 reflections with I > 2σ(I)
graphiteRint = 0.029
Detector resolution: 13.6612 pixels mm-1θmax = 26.0°, θmin = 3.0°
ω scansh = −9→9
Absorption correction: multi-scan (CrystalClear; Rigaku, 2005)k = −12→12
Tmin = 0.960, Tmax = 0.970l = −14→14
6950 measured reflections