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Bruker SMART APEX CCD area-detector diffractometer3799 independent reflections
Radiation source: fine-focus sealed tube2110 reflections with I > 2σ(I)
graphiteRint = 0.025
[var phi] and ω scansθmax = 35.4°, θmin = 2.4°
Absorption correction: multi-scan (SADABS; Sheldrick, 2000)h = −12→12
Tmin = 0.881, Tmax = 0.997k = −10→10
12290 measured reflectionsl = −27→26