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Bruker SMART CCD area-detector diffractometer4932 independent reflections
Radiation source: fine-focus sealed tube2127 reflections with I > 2σ(I)
Monochromator: graphiteRint = 0.121
T = 293(2) Kθmax = 26.5º
[var phi] and O scansθmin = 1.6º
Absorption correction: multi-scan(SADABS; Sheldrick, 1996)h = −9→9
Tmin = 0.700, Tmax = 0.884k = −21→14
13731 measured reflectionsl = −22→18