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Stoe IPDSII diffractometer4374 independent reflections
Radiation source: fine-focus sealed tube4327 reflections with I > 2σ(I)
Monochromator: graphiteRint = 0.064
Detector resolution: 0.15 mm pixels mm-1θmax = 29.2º
T = 120(2) Kθmin = 1.9º
rotation method scansh = −7→9
Absorption correction: Numerical(X-SHAPE and X-RED; Stoe & Cie, 2005)k = −20→17
Tmin = 0.070, Tmax = 0.270l = −22→22
9336 measured reflections