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Acta Crystallogr Sect E Struct Rep Online. 2008 March 1; 64(Pt 3): m474–m475.
Published online 2008 February 15. doi:  10.1107/S1600536808004182
PMCID: PMC2960748

Ammonium tris­(tetra­ethyl­ammonium) hexa­cosa­oxidoocta­molybdate

Abstract

The structure of the title compound, NH4(C8H20N)3[Mo8O26], is built up by discrete cations and anions, with two formula units in the asymmetric unit. The β-octa­molybdate anions are linked to the ammonium cations via N—H(...)O hydrogen bonding involving terminal oxide groups and to the tetra­ethyl­ammonium cations via weak C—H(...)O inter­actions.

Related literature

For related literature, see: Böschen et al. (1974 [triangle]); Briceño & Atencio (2004 [triangle]); Chakrabarti & Natarajan (2002 [triangle]); Harrison et al. (1993 [triangle]); Hsieh et al. (1987 [triangle]); Lindqvist (1950 [triangle]); Liu & Guo (2007 [triangle]); Liu et al. (2006 [triangle], 2008 [triangle]); Nelson et al. (2006 [triangle], 2007 [triangle]); Niven et al. (1991 [triangle]); Rarig & Zubieta (2001 [triangle]); Román et al. (1994 [triangle]); Sun et al. (2006 [triangle]); Thorn et al. (2005 [triangle]); Wu et al. (2001 [triangle]); Xiao et al. (2005 [triangle]); Xu et al. (2003 [triangle]); Yan et al. (2003 [triangle]); Zhang et al. (2004 [triangle]).

An external file that holds a picture, illustration, etc.
Object name is e-64-0m474-scheme1.jpg

Experimental

Crystal data

  • NH4(C8H20N)3[Mo8O26]
  • M r = 1592.31
  • Monoclinic, An external file that holds a picture, illustration, etc.
Object name is e-64-0m474-efi1.jpg
  • a = 10.7154 (2) Å
  • b = 22.8873 (3) Å
  • c = 19.9338 (2) Å
  • β = 96.906 (8)°
  • V = 4853.23 (12) Å3
  • Z = 4
  • Mo Kα radiation
  • μ = 2.08 mm−1
  • T = 293 (2) K
  • 0.25 × 0.15 × 0.05 mm

Data collection

  • Nonius KappaCCD diffractometer
  • Absorption correction: none
  • 57681 measured reflections
  • 29087 independent reflections
  • 21795 reflections with I > 2σ(I)
  • R int = 0.074

Refinement

  • R[F 2 > 2σ(F 2)] = 0.048
  • wR(F 2) = 0.124
  • S = 1.01
  • 29087 reflections
  • 1117 parameters
  • 1 restraint
  • H-atom parameters constrained
  • Δρmax = 0.86 e Å−3
  • Δρmin = −1.29 e Å−3
  • Absolute structure: Flack (1983 [triangle]), with 13317 Friedel pairs
  • Flack parameter: 0.17 (4)

Data collection: KappaCCD Server Software (Nonius, 1998 [triangle]); cell refinement: DENZO and SCALEPACK (Otwinowski & Minor, 1997 [triangle]); data reduction: DENZO and SCALEPACK; program(s) used to solve structure: SIR2004 (Burla et al., 2005 [triangle]); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008 [triangle]); molecular graphics: ORTEP-3 (Farrugia, 1997 [triangle]) and PLATON (Spek, 2003 [triangle]); software used to prepare material for publication: WinGX (Farrugia, 1999 [triangle]).

Table 1
Hydrogen-bond geometry (Å, °)

Supplementary Material

Crystal structure: contains datablocks global, I. DOI: 10.1107/S1600536808004182/bt2676sup1.cif

Structure factors: contains datablocks I. DOI: 10.1107/S1600536808004182/bt2676Isup2.hkl

Additional supplementary materials: crystallographic information; 3D view; checkCIF report

Acknowledgments

The authors thank Dr M. Giorgi from LBS-UMR 6517, Faculté des Sciences et Techniques de Saint Jérôme, France, for providing diffraction facilities, and the Centre Universitaire de Khenchela for financial support.

supplementary crystallographic information

Comment

The physical properties of polyoxomolybdates, containing Mo(VI) have made them the subject of intense research works for many years (Lindqvist, 1950; Román et al., 1994; Yan et al., 2003; Zhang et al., 2004; Liu et al., 2006; Nelson et al., 2007). These materials are generally constructed from [MoOx] polyhedra sharing common vertices and edges with one another and forming large anionic architectures (Briceño & Atencio, 2004; Thorn et al., 2005).

The octamolybdates have been the focus of special attention owing to the presence of several structure types (Hsieh et al., 1987; Harrison et al., 1993; Rarig & Zubieta, 2001; Niven et al., 1991; Nelson et al., 2006). Several compounds consisting of octamolybdate anions have been reported (Böschen et al., 1974; Chakrabarti & Natarajan, 2002; Xu et al., 2003; Xiao et al., 2005).

The asymmetric unit of the title compound consists of two ammonium, six tetraethylammonium cations and two hexacosaoxaoctamolybdate anions (Fig. 1).

The structure of the anions, as described recently (Liu & Guo, 2007), is constructed from an array of eight edge-shared MoO6 octahedra with 14 O(t), six O(µ2), four O(µ3) and two O(µ5) atoms.

The Mo—O distances, ranging from 1.684 (1) to 2.478 (1) Å, agree with those reported for other [Mo8O26]4- anions in the literature (Liu et al., 2008; Sun et al., 2006; Wu et al., 2001) and can be grouped into four sets bridging groups [Mo—O(terminal) 1.684 (1)–1.720 (1) Å, Mo—O(µ2): 1.742 (1)–2.271 (1) Å, Mo—O(µ3): 1.938 (1)–2.336 (1) Å and Mo—O(µ5): 2.108 (1)–2.477 (1) Å.

Polyhedral octamolybdates are separated by ammonium cations (Fig. 2) creating chains running along the c axis. In the crystal structure, an extended array of weak intermolecular C—H···O hydrogen bonds stabilizes the crystal packing.

Experimental

Single crystals of the title compound are prepared from a mixture of (NH4)6Mo7O24.1.5H2O (137 mg, 1 mmol), (C2H5)4NCl.H2O (386 mg, 3 mmol) and 3 ml H2O, heated in a Teflon-lined steel autoclave inside a programmable electric furnace at 160°C for 2 days. After cooling the autoclave to room temperature for 48 h, colorless crystals were obtained, filtered, washed with H2O, EtOH, Et2OH and dried in air.

Refinement

The title compound crystallizes in the non centrosymmetric space group P21 but the structure shows pseudo-symmetry m, which is fulfilled for approximately 91% of the atoms. Refinement in a higher symmetric space group is not possible. H atoms bonded to C were refined as riding with C—H distances of 0.97 Å or 0.96 Å and Uiso(H) = 1.2Ueq(C) or Uiso(H) = 1.5Ueq(C), for CH2 and CH3 groups respectively. Hydrogen atoms of the ammonium cations were located in difference Fourier syntheses and refined as riding with Uiso(H) = 0.036 Å2.

Figures

Fig. 1.
Asymmetric unit of the title compound, showing 30% probability displacement ellipsoids and arbitrary spheres for H atoms.
Fig. 2.
A partial packing diagram of the title compound with N—H···O hydrogen bonds shown as dashed lines.

Crystal data

NH4(C8H20N)3[Mo8O26]F000 = 3120
Mr = 1592.31Dx = 2.179 Mg m3
Monoclinic, P21Mo Kα radiation λ = 0.71073 Å
Hall symbol: P 2ybCell parameters from 29087 reflections
a = 10.7154 (2) Åθ = 1.0–31.0º
b = 22.8873 (3) ŵ = 2.08 mm1
c = 19.9338 (2) ÅT = 293 (2) K
β = 96.906 (8)ºPrism, colourless
V = 4853.23 (12) Å30.25 × 0.15 × 0.05 mm
Z = 4

Data collection

Nonius KappaCCD diffractometer21795 reflections with I > 2σ(I)
Radiation source: fine-focus sealed tubeRint = 0.074
Monochromator: graphiteθmax = 31.0º
T = 293(2) Kθmin = 1.0º
ω/θ scansh = −15→12
Absorption correction: nonek = −31→33
57681 measured reflectionsl = −28→25
29087 independent reflections

Refinement

Refinement on F2Hydrogen site location: difference Fourier map
Least-squares matrix: fullH-atom parameters constrained
R[F2 > 2σ(F2)] = 0.048  w = 1/[σ2(Fo2) + (0.0616P)2] where P = (Fo2 + 2Fc2)/3
wR(F2) = 0.124(Δ/σ)max = 0.003
S = 1.01Δρmax = 0.86 e Å3
29087 reflectionsΔρmin = −1.29 e Å3
1117 parametersExtinction correction: none
1 restraintAbsolute structure: Flack (1983), with 13317 Friedel pairs
Primary atom site location: structure-invariant direct methodsFlack parameter: 0.17 (4)
Secondary atom site location: difference Fourier map

Special details

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.
Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2)

xyzUiso*/Ueq
C11B0.5900 (10)−0.0413 (4)−1.1150 (6)0.066 (3)
H11F0.6002−0.0562−1.15960.080*
H11G0.5827−0.0747−1.08580.080*
C12B0.4705 (11)−0.0079 (6)−1.1198 (6)0.090 (4)
H12F0.4019−0.0329−1.13670.135*
H12H0.47460.0245−1.15000.135*
H12G0.45760.0063−1.07590.135*
C17B0.8094 (10)−0.0531 (4)−1.0826 (6)0.062 (3)
H17G0.8087−0.0722−1.12610.074*
H17F0.7886−0.0824−1.05070.074*
C18B0.9424 (11)−0.0322 (5)−1.0604 (7)0.089 (4)
H18H0.9992−0.0647−1.05930.134*
H18F0.9466−0.0152−1.01610.134*
H18G0.9655−0.0034−1.09170.134*
C13B0.6950 (9)0.0206 (4)−1.0217 (5)0.051 (2)
H13G0.77330.0405−1.00690.061*
H13F0.62980.0501−1.02890.061*
C14B0.6647 (11)−0.0188 (5)−0.9654 (6)0.072 (3)
H14H0.65870.0040−0.92550.108*
H14F0.7300−0.0474−0.95620.108*
H14G0.5860−0.0382−0.97860.108*
C15B0.7342 (10)0.0402 (4)−1.1364 (4)0.056 (3)
H15F0.66140.0657−1.14210.067*
H15G0.80390.0629−1.11450.067*
C16B0.7648 (12)0.0237 (6)−1.2051 (5)0.081 (3)
H16F0.77650.0585−1.23060.121*
H16H0.69710.0012−1.22790.121*
H16G0.84070.0010−1.20080.121*
C37A0.8065 (8)0.5109 (4)−0.7215 (4)0.0412 (19)
H37C0.87830.4851−0.71170.049*
H37D0.73400.4867−0.73590.049*
C38A0.8300 (11)0.5503 (5)−0.7793 (5)0.069 (3)
H38C0.84310.5269−0.81790.103*
H38D0.90320.5737−0.76630.103*
H38E0.75860.5752−0.79060.103*
C33A0.6717 (9)0.5826 (4)−0.6681 (5)0.063 (3)
H33C0.66290.6025−0.62590.076*
H33D0.68940.6122−0.70060.076*
C34A0.5496 (10)0.5544 (5)−0.6928 (6)0.079 (3)
H34E0.48550.5838−0.70070.119*
H34D0.52740.5273−0.65950.119*
H34C0.55720.5340−0.73420.119*
C31A0.7639 (10)0.4937 (4)−0.6057 (4)0.055 (2)
H31C0.69350.4697−0.62420.066*
H31D0.83790.4690−0.59980.066*
C32A0.7386 (13)0.5163 (6)−0.5368 (5)0.095 (4)
H32C0.72530.4839−0.50800.143*
H32D0.66520.5407−0.54200.143*
H32E0.80950.5387−0.51710.143*
C35A0.8932 (10)0.5803 (4)−0.6292 (5)0.068 (3)
H35C0.87830.5944−0.58500.081*
H35D0.89510.6140−0.65860.081*
C36A1.0221 (10)0.5509 (5)−0.6228 (6)0.093 (4)
H36D1.08530.5783−0.60490.139*
H36E1.03960.5380−0.66650.139*
H36C1.02240.5180−0.59300.139*
C31B0.7787 (12)0.4874 (5)−1.1157 (5)0.073 (3)
H31F0.70460.4664−1.13550.088*
H31G0.84960.4609−1.11460.088*
C32B0.7615 (14)0.5032 (7)−1.0450 (7)0.117 (5)
H32F0.74630.4685−1.02020.176*
H32G0.69120.5292−1.04520.176*
H32H0.83600.5222−1.02390.176*
C36B1.0417 (10)0.5365 (6)−1.1401 (6)0.090 (4)
H36G1.11210.5606−1.12360.135*
H36H1.04880.5250−1.18580.135*
H36F1.04080.5023−1.11230.135*
C35B0.9245 (10)0.5695 (6)−1.1379 (7)0.099 (4)
H35F0.92980.6047−1.16450.119*
H35G0.92120.5816−1.09160.119*
C33B0.7009 (11)0.5859 (5)−1.1646 (7)0.082 (4)
H33F0.70560.6041−1.12040.099*
H33G0.71900.6157−1.19650.099*
C34B0.5712 (10)0.5651 (6)−1.1835 (8)0.101 (5)
H34H0.51440.5977−1.18520.152*
H34G0.54970.5375−1.15050.152*
H34F0.56490.5467−1.22700.152*
C38B0.8294 (12)0.5536 (6)−1.2869 (6)0.099 (5)
H38F0.82900.5321−1.32830.149*
H38G0.91020.5715−1.27550.149*
H38H0.76570.5832−1.29240.149*
C37B0.8032 (9)0.5122 (4)−1.2306 (5)0.057 (3)
H37G0.72250.4936−1.24360.069*
H37F0.86660.4817−1.22680.069*
C26B0.6949 (9)0.3370 (6)−0.9758 (6)0.098 (5)
H26H0.62450.3564−1.00070.148*
H26F0.73300.3112−1.00550.148*
H26G0.75540.3655−0.95760.148*
C25B0.6511 (6)0.3026 (3)−0.9195 (3)0.0489 (17)
H25G0.58890.2746−0.93890.059*
H25F0.60910.3291−0.89160.059*
C27B0.6876 (7)0.2404 (4)−0.8198 (4)0.061 (2)
H27F0.62050.2161−0.84150.073*
H27G0.64920.2706−0.79490.073*
C28B0.7712 (11)0.2031 (7)−0.7696 (6)0.109 (5)
H28G0.72180.1865−0.73730.163*
H28F0.83670.2269−0.74660.163*
H28H0.80800.1722−0.79340.163*
C21B0.8170 (7)0.2264 (4)−0.9148 (4)0.056 (2)
H21F0.88320.2068−0.88580.067*
H21G0.85610.2476−0.94890.067*
C22B0.7296 (10)0.1811 (7)−0.9492 (7)0.118 (5)
H22G0.77590.1555−0.97540.177*
H22H0.66420.2001−0.97840.177*
H22F0.69310.1587−0.91570.177*
C23B0.8546 (6)0.3111 (4)−0.8435 (4)0.0550 (19)
H23F0.91850.2889−0.81590.066*
H23G0.89390.3282−0.88030.066*
C25A−0.1879 (7)0.2949 (4)−0.4261 (4)0.065 (2)
H25D−0.14480.2662−0.45080.078*
H25C−0.12500.3213−0.40390.078*
C26A−0.2785 (12)0.3297 (7)−0.4761 (7)0.124 (6)
H26E−0.23250.3484−0.50860.186*
H26D−0.32010.3588−0.45210.186*
H26C−0.33990.3038−0.49900.186*
C27A−0.1540 (6)0.2306 (4)−0.3304 (3)0.0507 (18)
H27D−0.09030.2578−0.31090.061*
H27C−0.11430.2040−0.35930.061*
C28A−0.2019 (11)0.1955 (6)−0.2736 (6)0.092 (4)
H28D−0.13280.1756−0.24820.139*
H28E−0.26270.1674−0.29250.139*
H28C−0.24040.2215−0.24430.139*
C21A−0.3582 (7)0.2250 (4)−0.4049 (4)0.059 (2)
H21C−0.40100.2079−0.36940.070*
H21D−0.41850.2492−0.43240.070*
C22A−0.3181 (9)0.1771 (6)−0.4477 (7)0.114 (5)
H22D−0.39030.1548−0.46590.171*
H22C−0.26000.1521−0.42090.171*
H22E−0.27820.1933−0.48400.171*
C23A−0.3159 (7)0.3067 (4)−0.3295 (4)0.0575 (19)
H23C−0.35910.2848−0.29760.069*
H23D−0.37910.3281−0.35860.069*
C15A0.7166 (12)0.0417 (4)−0.6414 (5)0.070 (3)
H15C0.64060.0651−0.64550.084*
H15D0.78530.0669−0.62320.084*
C16A0.7398 (15)0.0239 (6)−0.7106 (6)0.111 (5)
H16C0.74290.0580−0.73840.167*
H16E0.6732−0.0012−0.72980.167*
H16D0.81840.0034−0.70830.167*
C11A0.5875 (13)−0.0434 (4)−0.6125 (7)0.089 (4)
H11C0.5995−0.0625−0.65460.106*
H11D0.5840−0.0738−0.57880.106*
C12A0.4644 (12)−0.0134 (7)−0.6217 (6)0.101 (4)
H12C0.3991−0.0414−0.63430.152*
H12E0.46430.0156−0.65660.152*
H12D0.44980.0052−0.58020.152*
C13A0.6887 (11)0.0267 (5)−0.5263 (5)0.064 (3)
H13D0.61750.0530−0.53480.077*
H13C0.76300.0506−0.51470.077*
C14A0.6698 (12)−0.0111 (5)−0.4652 (6)0.087 (4)
H14E0.66200.0136−0.42700.131*
H14C0.7407−0.0366−0.45520.131*
H14D0.5948−0.0340−0.47510.131*
C17A0.8105 (12)−0.0467 (6)−0.5868 (8)0.095 (4)
H17D0.8079−0.0670−0.62960.114*
H17C0.7995−0.0756−0.55250.114*
C18A0.9391 (14)−0.0192 (7)−0.5705 (8)0.128 (6)
H18E1.0026−0.0488−0.57110.192*
H18C0.9455−0.0017−0.52650.192*
H18D0.95070.0101−0.60350.192*
C24B0.8107 (10)0.3601 (6)−0.8011 (7)0.120 (6)
H24F0.88110.3842−0.78460.180*
H24H0.77410.3439−0.76350.180*
H24G0.74920.3832−0.82810.180*
C24A−0.2284 (10)0.3512 (6)−0.2896 (7)0.106 (4)
H24C−0.27710.3764−0.26420.159*
H24D−0.18670.3742−0.32040.159*
H24E−0.16700.3309−0.25920.159*
O63A0.4350 (4)0.2364 (2)−0.5727 (2)0.0240 (10)
O63B0.4454 (4)0.2441 (2)−1.0729 (2)0.0251 (10)
O33A0.0596 (4)0.3021 (2)−0.6769 (2)0.0293 (11)
O84B0.0628 (5)0.1691 (2)−1.1462 (2)0.0319 (11)
O33B0.0529 (4)0.2868 (2)−1.1749 (2)0.0277 (11)
O82A0.2989 (5)0.2895 (2)−0.6797 (2)0.0260 (11)
O83A0.2917 (4)0.1778 (2)−0.6589 (2)0.0273 (10)
O83B0.3178 (5)0.1763 (2)−1.1557 (2)0.0275 (10)
O72A0.1962 (4)0.2486 (2)−0.5683 (2)0.0236 (11)
O82B0.2924 (5)0.2873 (2)−1.1802 (2)0.0244 (10)
O21A0.0558 (5)0.1961 (2)−0.4558 (2)0.0399 (13)
O74B0.4374 (4)0.3622 (2)−1.1003 (2)0.0291 (10)
O22A−0.0928 (5)0.1334 (2)−0.5480 (3)0.0475 (13)
O42B0.1132 (5)0.3393 (3)−1.2918 (2)0.0411 (13)
O73A0.2035 (5)0.3600 (2)−0.5897 (2)0.0263 (10)
O72B0.2058 (4)0.2430 (2)−1.0658 (2)0.0225 (10)
O51A0.4373 (5)0.3422 (3)−0.7930 (3)0.0415 (13)
O73B0.1823 (4)0.3543 (2)−1.0915 (2)0.0246 (9)
O32B0.0710 (5)0.3227 (3)−0.9782 (2)0.0373 (13)
O41A0.0695 (5)0.4257 (2)−0.6961 (3)0.0434 (13)
O31B−0.0832 (5)0.3561 (2)−1.0875 (2)0.0443 (13)
O52A0.5870 (5)0.4049 (2)−0.7032 (3)0.0484 (14)
O84A0.0366 (4)0.1842 (2)−0.6525 (2)0.0319 (11)
O13A0.1705 (4)0.1343 (2)−0.5490 (2)0.0324 (11)
O22B−0.0431 (5)0.1136 (2)−1.0348 (3)0.0478 (14)
O43A0.3238 (5)0.4046 (2)−0.6998 (2)0.0328 (11)
O23A−0.0547 (5)0.2549 (2)−0.5672 (2)0.0322 (11)
O62B0.4271 (5)0.2088 (3)−1.2696 (3)0.0417 (14)
O42A0.1404 (5)0.3521 (3)−0.7901 (2)0.0393 (13)
O81B0.1379 (5)0.2055 (2)−1.2653 (2)0.0328 (12)
O11A0.4260 (5)0.1128 (2)−0.5524 (3)0.0423 (13)
O61A0.5559 (5)0.1622 (2)−0.6610 (3)0.0455 (13)
O62A0.4122 (5)0.2059 (2)−0.7701 (3)0.0391 (13)
O12B0.3875 (5)0.1922 (3)−0.9539 (2)0.0391 (12)
O52B0.5442 (5)0.4169 (2)−1.2100 (3)0.0456 (13)
O41B0.0283 (5)0.4094 (2)−1.1990 (3)0.0432 (13)
O71A0.3722 (5)0.3209 (3)−0.4789 (2)0.0362 (12)
O71B0.3627 (5)0.3265 (2)−0.9816 (2)0.0328 (12)
O32A0.0814 (5)0.3313 (3)−0.4784 (3)0.0393 (13)
O51B0.4086 (5)0.3439 (3)−1.2959 (3)0.0433 (13)
O53A0.5489 (4)0.2832 (2)−0.6818 (3)0.0306 (11)
O74A0.4590 (5)0.3546 (2)−0.5951 (2)0.0301 (10)
O23B−0.0423 (5)0.2361 (2)−1.0614 (2)0.0318 (11)
O12A0.3559 (5)0.1859 (3)−0.4581 (2)0.0406 (13)
O53B0.5426 (4)0.2943 (2)−1.1851 (3)0.0317 (11)
O61B0.5830 (5)0.1748 (3)−1.1601 (3)0.0466 (13)
O81A0.1240 (5)0.2178 (2)−0.7693 (2)0.0363 (12)
O31A−0.0594 (5)0.3763 (2)−0.5860 (3)0.0469 (14)
O11B0.4731 (5)0.1207 (2)−1.0460 (3)0.0448 (14)
O21B0.0913 (5)0.1883 (2)−0.9499 (2)0.0374 (12)
O13B0.2153 (5)0.1291 (2)−1.0418 (2)0.0343 (11)
O43B0.2849 (5)0.4023 (2)−1.2039 (2)0.0342 (11)
Mo8B0.16071 (6)0.21879 (2)−1.18123 (3)0.02338 (12)
Mo6B0.46244 (6)0.22070 (3)−1.18465 (3)0.02825 (13)
Mo8A0.14772 (6)0.22861 (2)−0.68488 (3)0.02326 (13)
Mo7A0.34782 (6)0.30996 (3)−0.56384 (3)0.02454 (12)
Mo7B0.33886 (6)0.31190 (2)−1.06563 (3)0.02297 (12)
Mo5B0.44034 (6)0.36111 (3)−1.21243 (3)0.03065 (14)
Mo3A0.04691 (6)0.32317 (3)−0.56325 (3)0.02823 (14)
Mo3B0.03669 (6)0.31022 (3)−1.06231 (3)0.02674 (13)
Mo2A0.02633 (6)0.18241 (3)−0.54103 (3)0.02875 (13)
Mo2B0.05973 (6)0.17012 (3)−1.03372 (3)0.02931 (13)
Mo6A0.44880 (6)0.21524 (2)−0.68482 (3)0.02695 (13)
Mo4A0.16441 (6)0.36812 (2)−0.70606 (3)0.02810 (13)
Mo5A0.46756 (6)0.35566 (3)−0.70857 (3)0.02927 (13)
Mo4B0.13666 (6)0.35758 (2)−1.20848 (3)0.02786 (13)
Mo1A0.33042 (6)0.17053 (2)−0.54277 (3)0.02758 (13)
Mo1B0.36327 (6)0.17345 (2)−1.03793 (3)0.02745 (13)
N1B0.7074 (7)−0.0082 (3)−1.0889 (4)0.0454 (17)
N3A0.7839 (7)0.5418 (3)−0.6566 (4)0.0444 (17)
N3B0.8013 (8)0.5396 (3)−1.1623 (4)0.059 (2)
N2B0.7529 (7)0.2690 (4)−0.8734 (4)0.0378 (10)
N2A−0.2534 (7)0.2637 (4)−0.3725 (4)0.0391 (12)
N1A0.7031 (8)−0.0053 (3)−0.5909 (4)0.060 (2)
N4A0.2511 (8)0.2697 (4)−0.8729 (4)0.0364 (10)
N4B0.2417 (8)0.2655 (4)−1.3738 (4)0.0364 (11)
H1N0.24500.2606−0.91280.036*
H2N0.28050.3089−0.86560.036*
H3N0.30510.2519−0.85960.036*
H4N0.18320.2583−0.84860.036*
H5N0.23010.2638−1.41640.036*
H6N0.30100.2356−1.36060.036*
H7N0.17230.2543−1.34970.036*
H8N0.26960.3050−1.36680.036*

Atomic displacement parameters (Å2)

U11U22U33U12U13U23
C11B0.075 (6)0.034 (4)0.085 (6)−0.012 (4)−0.015 (5)−0.015 (4)
C12B0.076 (8)0.092 (9)0.096 (8)−0.023 (7)−0.014 (6)−0.024 (7)
C17B0.069 (6)0.033 (4)0.085 (7)0.016 (4)0.018 (5)−0.010 (4)
C18B0.063 (6)0.053 (6)0.153 (11)0.026 (5)0.015 (7)−0.013 (7)
C13B0.054 (6)0.039 (5)0.056 (5)0.005 (4)−0.002 (4)0.001 (4)
C14B0.077 (8)0.052 (6)0.091 (8)−0.009 (6)0.028 (6)0.007 (5)
C15B0.083 (7)0.031 (4)0.052 (5)−0.012 (4)0.000 (4)−0.011 (4)
C16B0.124 (9)0.057 (6)0.061 (6)−0.003 (6)0.010 (6)−0.005 (5)
C37A0.047 (5)0.022 (3)0.054 (4)0.000 (3)0.001 (4)−0.012 (3)
C38A0.075 (7)0.063 (6)0.065 (6)−0.012 (6)−0.003 (5)0.013 (5)
C33A0.069 (6)0.037 (5)0.078 (6)0.024 (4)−0.011 (5)−0.012 (4)
C34A0.055 (6)0.073 (7)0.103 (8)0.025 (5)−0.017 (5)−0.012 (6)
C31A0.072 (6)0.039 (5)0.052 (5)0.008 (4)0.002 (4)−0.001 (4)
C32A0.144 (11)0.087 (9)0.056 (6)0.000 (9)0.018 (7)−0.012 (6)
C35A0.080 (7)0.040 (5)0.076 (6)−0.014 (5)−0.019 (5)−0.008 (4)
C36A0.070 (7)0.065 (7)0.131 (10)−0.012 (6)−0.042 (7)0.011 (7)
C31B0.097 (8)0.038 (5)0.080 (7)0.023 (5)−0.012 (6)−0.013 (5)
C32B0.125 (12)0.122 (12)0.103 (10)0.034 (10)0.006 (8)−0.008 (9)
C36B0.060 (6)0.081 (8)0.121 (9)0.010 (6)−0.019 (6)−0.040 (7)
C35B0.068 (7)0.076 (8)0.143 (11)0.004 (6)−0.030 (7)−0.041 (7)
C33B0.086 (8)0.034 (5)0.127 (10)0.013 (5)0.011 (7)0.000 (6)
C34B0.054 (6)0.064 (7)0.184 (14)0.010 (5)0.004 (7)0.027 (8)
C38B0.100 (10)0.081 (9)0.107 (9)0.009 (8)−0.025 (7)0.048 (7)
C37B0.058 (6)0.035 (5)0.072 (6)0.011 (4)−0.023 (5)−0.013 (4)
C26B0.046 (5)0.133 (12)0.114 (9)−0.022 (6)−0.003 (5)0.059 (8)
C25B0.031 (3)0.065 (5)0.048 (4)−0.001 (3)−0.004 (3)0.010 (4)
C27B0.043 (4)0.084 (7)0.061 (5)0.013 (4)0.024 (4)0.016 (4)
C28B0.081 (8)0.162 (13)0.091 (8)0.057 (8)0.040 (6)0.079 (8)
C21B0.040 (4)0.060 (5)0.071 (5)−0.003 (4)0.022 (3)−0.023 (4)
C22B0.072 (8)0.110 (10)0.176 (12)−0.011 (8)0.027 (8)−0.087 (10)
C23B0.032 (4)0.065 (5)0.064 (5)0.009 (4)−0.008 (3)−0.009 (4)
C25A0.043 (4)0.091 (7)0.067 (5)0.015 (4)0.028 (4)0.025 (5)
C26A0.084 (8)0.170 (15)0.127 (11)0.045 (9)0.051 (8)0.094 (10)
C27A0.032 (4)0.066 (5)0.053 (4)0.006 (3)0.005 (3)−0.007 (4)
C28A0.087 (8)0.108 (10)0.079 (7)0.007 (7)0.001 (6)0.055 (7)
C21A0.040 (4)0.062 (5)0.070 (5)0.006 (4)−0.009 (3)−0.018 (4)
C22A0.057 (7)0.111 (10)0.166 (11)0.032 (7)−0.022 (7)−0.077 (9)
C23A0.045 (4)0.065 (5)0.065 (5)0.003 (4)0.016 (3)−0.007 (4)
C15A0.094 (8)0.034 (4)0.075 (6)0.004 (5)−0.016 (6)−0.010 (4)
C16A0.186 (15)0.070 (8)0.078 (8)0.014 (9)0.013 (8)−0.021 (6)
C11A0.124 (10)0.028 (5)0.105 (8)−0.010 (6)−0.020 (7)−0.023 (5)
C12A0.093 (9)0.104 (10)0.102 (9)−0.036 (8)−0.013 (7)−0.033 (8)
C13A0.070 (7)0.048 (6)0.071 (6)0.002 (5)−0.007 (5)0.001 (5)
C14A0.096 (9)0.061 (7)0.105 (9)0.001 (7)0.013 (7)0.005 (7)
C17A0.093 (9)0.060 (7)0.137 (11)0.042 (7)0.034 (8)0.007 (7)
C18A0.089 (10)0.128 (13)0.164 (14)0.037 (9)0.002 (9)0.026 (10)
C24B0.076 (7)0.120 (11)0.152 (11)0.030 (8)−0.033 (7)−0.095 (10)
C24A0.062 (7)0.098 (9)0.161 (11)−0.018 (7)0.027 (7)−0.068 (8)
O63A0.024 (2)0.021 (2)0.027 (2)−0.0004 (17)0.0073 (17)0.0003 (16)
O63B0.024 (2)0.024 (2)0.027 (2)0.0006 (17)0.0062 (18)0.0040 (16)
O33A0.025 (2)0.023 (2)0.039 (3)0.0057 (19)0.0019 (19)0.0062 (19)
O84B0.033 (2)0.030 (2)0.032 (2)−0.003 (2)0.0007 (18)0.0052 (19)
O33B0.027 (2)0.025 (2)0.031 (2)−0.0007 (19)0.0002 (18)−0.0007 (17)
O82A0.029 (3)0.021 (2)0.029 (3)0.002 (2)0.007 (2)0.0037 (18)
O83A0.027 (2)0.022 (2)0.034 (2)−0.0004 (19)0.0079 (17)−0.0006 (18)
O83B0.032 (2)0.020 (2)0.031 (2)0.0044 (19)0.0050 (17)−0.0010 (18)
O72A0.025 (2)0.025 (2)0.021 (2)0.0009 (19)0.0013 (18)0.0002 (17)
O82B0.028 (2)0.020 (2)0.026 (2)0.0005 (19)0.0077 (19)0.0023 (16)
O21A0.049 (3)0.038 (3)0.035 (3)0.001 (2)0.012 (2)0.008 (2)
O74B0.033 (2)0.025 (2)0.030 (2)−0.0071 (19)0.0081 (17)−0.0047 (17)
O22A0.046 (3)0.039 (3)0.059 (3)−0.010 (2)0.016 (2)0.006 (2)
O42B0.050 (3)0.043 (3)0.031 (2)0.007 (2)0.007 (2)0.008 (2)
O73A0.032 (2)0.017 (2)0.032 (2)0.0013 (18)0.0085 (17)−0.0016 (17)
O72B0.027 (2)0.019 (2)0.022 (2)−0.0033 (19)0.0052 (18)−0.0002 (15)
O51A0.049 (3)0.041 (3)0.035 (3)−0.001 (2)0.009 (2)0.006 (2)
O73B0.030 (2)0.016 (2)0.029 (2)−0.0002 (18)0.0079 (16)−0.0002 (17)
O32B0.041 (3)0.038 (3)0.034 (3)−0.001 (2)0.012 (2)−0.006 (2)
O41A0.044 (3)0.035 (3)0.053 (3)0.012 (2)0.014 (2)0.009 (2)
O31B0.045 (3)0.044 (3)0.045 (3)0.009 (3)0.010 (2)0.010 (2)
O52A0.049 (3)0.039 (3)0.059 (3)−0.021 (2)0.010 (2)−0.003 (2)
O84A0.032 (2)0.028 (2)0.037 (2)−0.002 (2)0.0071 (18)0.0022 (19)
O13A0.039 (3)0.019 (2)0.041 (2)0.005 (2)0.009 (2)0.0049 (17)
O22B0.047 (3)0.044 (3)0.055 (3)−0.013 (2)0.015 (2)0.005 (2)
O43A0.041 (3)0.024 (2)0.035 (2)−0.001 (2)0.0079 (19)0.0022 (18)
O23A0.032 (2)0.030 (3)0.036 (2)−0.002 (2)0.007 (2)0.0015 (19)
O62B0.049 (3)0.041 (3)0.039 (3)−0.003 (3)0.017 (2)−0.006 (2)
O42A0.041 (3)0.047 (3)0.030 (2)0.002 (2)0.0039 (19)0.006 (2)
O81B0.036 (3)0.035 (3)0.028 (2)−0.003 (2)0.0022 (19)−0.0008 (19)
O11A0.047 (3)0.033 (3)0.048 (3)0.007 (2)0.010 (2)0.010 (2)
O61A0.041 (3)0.033 (3)0.066 (3)0.010 (2)0.018 (2)0.009 (2)
O62A0.049 (3)0.031 (3)0.039 (3)−0.006 (2)0.013 (2)−0.004 (2)
O12B0.045 (3)0.041 (3)0.032 (2)0.001 (2)0.005 (2)0.009 (2)
O52B0.049 (3)0.036 (3)0.054 (3)−0.012 (2)0.011 (2)0.004 (2)
O41B0.050 (3)0.028 (3)0.052 (3)0.016 (2)0.008 (2)0.007 (2)
O71A0.039 (3)0.041 (3)0.029 (2)0.000 (2)0.006 (2)−0.006 (2)
O71B0.035 (3)0.034 (3)0.030 (2)0.001 (2)0.006 (2)−0.0023 (19)
O32A0.048 (3)0.040 (3)0.033 (3)0.003 (3)0.015 (2)−0.002 (2)
O51B0.056 (3)0.042 (3)0.034 (3)0.005 (3)0.011 (2)0.006 (2)
O53A0.024 (2)0.030 (2)0.038 (3)0.0036 (19)0.0071 (19)−0.0018 (18)
O74A0.036 (2)0.027 (2)0.029 (2)−0.009 (2)0.0059 (17)−0.0055 (18)
O23B0.031 (2)0.031 (2)0.035 (2)−0.009 (2)0.0106 (19)−0.0003 (19)
O12A0.049 (3)0.043 (3)0.030 (2)0.003 (2)0.006 (2)0.011 (2)
O53B0.026 (2)0.032 (2)0.039 (3)0.0034 (19)0.0110 (19)0.0025 (19)
O61B0.038 (3)0.040 (3)0.064 (3)0.014 (2)0.016 (2)0.004 (2)
O81A0.042 (3)0.036 (3)0.031 (2)−0.004 (2)0.005 (2)0.002 (2)
O31A0.048 (3)0.041 (3)0.054 (3)0.013 (3)0.018 (2)0.015 (2)
O11B0.043 (3)0.038 (3)0.052 (3)0.018 (2)0.004 (2)0.006 (2)
O21B0.046 (3)0.037 (3)0.032 (2)−0.005 (2)0.011 (2)0.006 (2)
O13B0.042 (3)0.020 (2)0.041 (3)−0.002 (2)0.007 (2)0.0065 (18)
O43B0.041 (3)0.027 (2)0.036 (2)0.002 (2)0.012 (2)0.0104 (18)
Mo8B0.0270 (3)0.0207 (3)0.0225 (3)−0.0004 (2)0.0030 (2)−0.0018 (2)
Mo6B0.0306 (3)0.0261 (3)0.0298 (3)0.0032 (2)0.0105 (2)0.0000 (2)
Mo8A0.0264 (3)0.0210 (3)0.0224 (3)−0.0009 (2)0.0030 (2)−0.0005 (2)
Mo7A0.0288 (3)0.0222 (3)0.0226 (3)−0.0008 (2)0.0030 (2)−0.0018 (2)
Mo7B0.0260 (3)0.0204 (2)0.0226 (3)−0.0012 (2)0.0030 (2)−0.0008 (2)
Mo5B0.0348 (3)0.0273 (3)0.0314 (3)−0.0043 (3)0.0104 (2)0.0050 (2)
Mo3A0.0317 (3)0.0230 (3)0.0318 (3)0.0043 (2)0.0112 (2)0.0006 (2)
Mo3B0.0278 (3)0.0247 (3)0.0291 (3)0.0021 (2)0.0088 (2)0.0007 (2)
Mo2A0.0308 (3)0.0250 (3)0.0317 (3)−0.0031 (2)0.0088 (2)0.0037 (2)
Mo2B0.0332 (3)0.0248 (3)0.0311 (3)−0.0058 (2)0.0087 (2)0.0031 (2)
Mo6A0.0297 (3)0.0225 (3)0.0304 (3)0.0024 (2)0.0108 (2)0.0003 (2)
Mo4A0.0326 (3)0.0226 (3)0.0297 (3)0.0047 (2)0.0060 (2)0.0066 (2)
Mo5A0.0335 (3)0.0238 (3)0.0319 (3)−0.0051 (2)0.0095 (2)0.0009 (2)
Mo4B0.0321 (3)0.0242 (3)0.0276 (3)0.0052 (2)0.0049 (2)0.0056 (2)
Mo1A0.0307 (3)0.0237 (3)0.0288 (3)0.0043 (2)0.0054 (2)0.0070 (2)
Mo1B0.0312 (3)0.0230 (3)0.0283 (3)0.0049 (2)0.0042 (2)0.0055 (2)
N1B0.048 (4)0.024 (3)0.061 (4)0.002 (3)−0.004 (3)−0.011 (3)
N3A0.054 (4)0.024 (3)0.053 (4)0.001 (3)−0.004 (3)−0.010 (3)
N3B0.071 (6)0.028 (4)0.075 (5)0.005 (4)−0.007 (4)−0.013 (4)
N2B0.028 (2)0.044 (3)0.043 (3)0.0034 (19)0.0096 (18)−0.003 (2)
N2A0.026 (2)0.049 (3)0.044 (3)0.004 (2)0.0108 (19)0.000 (2)
N1A0.064 (5)0.031 (4)0.079 (5)0.016 (4)−0.016 (4)−0.020 (4)
N4A0.048 (3)0.041 (3)0.021 (2)−0.002 (2)0.0058 (18)−0.0018 (18)
N4B0.049 (3)0.036 (3)0.025 (2)0.001 (2)0.0092 (19)0.0042 (18)

Geometric parameters (Å, °)

C11B—C12B1.484 (15)C15A—H15C0.9700
C11B—N1B1.506 (12)C15A—H15D0.9700
C11B—H11F0.9700C16A—H16C0.9600
C11B—H11G0.9700C16A—H16E0.9600
C12B—H12F0.9600C16A—H16D0.9600
C12B—H12H0.9600C11A—C12A1.479 (17)
C12B—H12G0.9600C11A—N1A1.534 (14)
C17B—N1B1.494 (12)C11A—H11C0.9700
C17B—C18B1.518 (16)C11A—H11D0.9700
C17B—H17G0.9700C12A—H12C0.9600
C17B—H17F0.9700C12A—H12E0.9600
C18B—H18H0.9600C12A—H12D0.9600
C18B—H18F0.9600C13A—N1A1.505 (13)
C18B—H18G0.9600C13A—C14A1.527 (15)
C13B—C14B1.506 (13)C13A—H13D0.9700
C13B—N1B1.512 (11)C13A—H13C0.9700
C13B—H13G0.9700C14A—H14E0.9600
C13B—H13F0.9700C14A—H14C0.9600
C14B—H14H0.9600C14A—H14D0.9600
C14B—H14F0.9600C17A—N1A1.485 (14)
C14B—H14G0.9600C17A—C18A1.513 (19)
C15B—C16B1.494 (13)C17A—H17D0.9700
C15B—N1B1.506 (11)C17A—H17C0.9700
C15B—H15F0.9700C18A—H18E0.9600
C15B—H15G0.9700C18A—H18C0.9600
C16B—H16F0.9600C18A—H18D0.9600
C16B—H16H0.9600C24B—H24F0.9600
C16B—H16G0.9600C24B—H24H0.9600
C37A—C38A1.508 (12)C24B—H24G0.9600
C37A—N3A1.518 (10)C24A—H24C0.9600
C37A—H37C0.9700C24A—H24D0.9600
C37A—H37D0.9700C24A—H24E0.9600
C38A—H38C0.9600O63A—Mo7A1.944 (5)
C38A—H38D0.9600O63A—Mo1A2.010 (4)
C38A—H38E0.9600O63A—Mo6A2.310 (4)
C33A—C34A1.489 (14)O63B—Mo7B1.943 (5)
C33A—N3A1.519 (12)O63B—Mo1B2.005 (5)
C33A—H33C0.9700O63B—Mo6B2.320 (4)
C33A—H33D0.9700O33A—Mo8A1.946 (5)
C34A—H34E0.9600O33A—Mo4A2.010 (5)
C34A—H34D0.9600O33A—Mo3A2.336 (5)
C34A—H34C0.9600O84B—Mo8B1.749 (5)
C31A—C32A1.522 (13)O84B—Mo2B2.246 (4)
C31A—N3A1.529 (11)O33B—Mo8B1.952 (5)
C31A—H31C0.9700O33B—Mo4B2.005 (5)
C31A—H31D0.9700O33B—Mo3B2.334 (5)
C32A—H32C0.9600O82A—Mo8A2.130 (5)
C32A—H32D0.9600O82A—Mo4A2.326 (5)
C32A—H32E0.9600O82A—Mo6A2.349 (5)
C35A—N3A1.515 (11)O82A—Mo7A2.353 (5)
C35A—C36A1.528 (14)O82A—Mo5A2.478 (5)
C35A—H35C0.9700O83A—Mo8A1.951 (5)
C35A—H35D0.9700O83A—Mo6A2.011 (5)
C36A—H36D0.9600O83A—Mo1A2.309 (4)
C36A—H36E0.9600O83B—Mo8B1.958 (5)
C36A—H36C0.9600O83B—Mo6B1.995 (5)
C31B—C32B1.489 (14)O83B—Mo1B2.340 (4)
C31B—N3B1.550 (13)O72A—Mo7A2.142 (5)
C31B—H31F0.9700O72A—Mo1A2.312 (5)
C31B—H31G0.9700O72A—Mo3A2.350 (5)
C32B—H32F0.9600O72A—Mo8A2.363 (4)
C32B—H32G0.9600O72A—Mo2A2.478 (5)
C32B—H32H0.9600O82B—Mo8B2.108 (5)
C36B—C35B1.470 (15)O82B—Mo4B2.338 (5)
C36B—H36G0.9600O82B—Mo7B2.347 (5)
C36B—H36H0.9600O82B—Mo6B2.385 (5)
C36B—H36F0.9600O82B—Mo5B2.454 (5)
C35B—N3B1.514 (13)O21A—Mo2A1.719 (5)
C35B—H35F0.9700O74B—Mo7B1.759 (5)
C35B—H35G0.9700O74B—Mo5B2.240 (4)
C33B—C34B1.474 (16)O22A—Mo2A1.692 (5)
C33B—N3B1.506 (14)O42B—Mo4B1.702 (5)
C33B—H33F0.9700O73A—Mo7A1.944 (5)
C33B—H33G0.9700O73A—Mo3A2.004 (5)
C34B—H34H0.9600O73A—Mo4A2.314 (4)
C34B—H34G0.9600O72B—Mo7B2.125 (5)
C34B—H34F0.9600O72B—Mo1B2.338 (5)
C38B—C37B1.520 (14)O72B—Mo8B2.359 (4)
C38B—H38F0.9600O72B—Mo3B2.384 (5)
C38B—H38G0.9600O72B—Mo2B2.426 (5)
C38B—H38H0.9600O51A—Mo5A1.704 (5)
C37B—N3B1.502 (11)O73B—Mo7B1.953 (5)
C37B—H37G0.9700O73B—Mo3B2.003 (5)
C37B—H37F0.9700O73B—Mo4B2.325 (4)
C26B—C25B1.492 (12)O32B—Mo3B1.697 (5)
C26B—H26H0.9600O41A—Mo4A1.691 (5)
C26B—H26F0.9600O31B—Mo3B1.688 (5)
C26B—H26G0.9600O52A—Mo5A1.700 (5)
C25B—N2B1.544 (10)O84A—Mo8A1.746 (5)
C25B—H25G0.9700O84A—Mo2A2.239 (4)
C25B—H25F0.9700O13A—Mo1A1.894 (5)
C27B—N2B1.498 (10)O13A—Mo2A1.919 (5)
C27B—C28B1.522 (12)O22B—Mo2B1.697 (5)
C27B—H27F0.9700O43A—Mo4A1.892 (5)
C27B—H27G0.9700O43A—Mo5A1.929 (5)
C28B—H28G0.9600O23A—Mo3A1.901 (5)
C28B—H28F0.9600O23A—Mo2A1.915 (5)
C28B—H28H0.9600O62B—Mo6B1.713 (5)
C21B—N2B1.498 (10)O42A—Mo4A1.704 (5)
C21B—C22B1.505 (13)O81B—Mo8B1.692 (5)
C21B—H21F0.9700O11A—Mo1A1.697 (5)
C21B—H21G0.9700O61A—Mo6A1.699 (5)
C22B—H22G0.9600O62A—Mo6A1.712 (5)
C22B—H22H0.9600O12B—Mo1B1.718 (5)
C22B—H22F0.9600O52B—Mo5B1.691 (5)
C23B—C24B1.513 (13)O41B—Mo4B1.686 (5)
C23B—N2B1.521 (11)O71A—Mo7A1.700 (5)
C23B—H23F0.9700O71B—Mo7B1.697 (5)
C23B—H23G0.9700O32A—Mo3A1.698 (5)
C25A—N2A1.524 (10)O51B—Mo5B1.705 (5)
C25A—C26A1.529 (13)O53A—Mo6A1.887 (5)
C25A—H25D0.9700O53A—Mo5A1.918 (5)
C25A—H25C0.9700O74A—Mo7A1.741 (5)
C26A—H26E0.9600O74A—Mo5A2.274 (4)
C26A—H26D0.9600O23B—Mo3B1.896 (5)
C26A—H26C0.9600O23B—Mo2B1.907 (5)
C27A—N2A1.483 (10)O12A—Mo1A1.713 (5)
C27A—C28A1.527 (12)O53B—Mo6B1.891 (5)
C27A—H27D0.9700O53B—Mo5B1.922 (5)
C27A—H27C0.9700O61B—Mo6B1.691 (5)
C28A—H28D0.9600O81A—Mo8A1.690 (5)
C28A—H28E0.9600O31A—Mo3A1.691 (5)
C28A—H28C0.9600O11B—Mo1B1.707 (5)
C21A—C22A1.484 (13)O21B—Mo2B1.716 (5)
C21A—N2A1.512 (11)O13B—Mo1B1.877 (5)
C21A—H21C0.9700O13B—Mo2B1.937 (5)
C21A—H21D0.9700O43B—Mo4B1.882 (5)
C22A—H22D0.9600O43B—Mo5B1.939 (5)
C22A—H22C0.9600N4A—H1N0.82
C22A—H22E0.9600N4A—H2N0.96
C23A—N2A1.514 (10)N4A—H3N0.73
C23A—C24A1.539 (13)N4A—H4N0.96
C23A—H23C0.9700N4B—H5N0.85
C23A—H23D0.9700N4B—H6N0.95
C15A—C16A1.488 (15)N4B—H7N0.97
C15A—N1A1.492 (13)N4B—H8N0.96
C12B—C11B—N1B116.2 (8)Mo8A—O72A—Mo2A90.99 (16)
C12B—C11B—H11F108.2Mo8B—O82B—Mo4B92.95 (19)
N1B—C11B—H11F108.2Mo8B—O82B—Mo7B104.55 (18)
C12B—C11B—H11G108.2Mo4B—O82B—Mo7B97.53 (19)
N1B—C11B—H11G108.2Mo8B—O82B—Mo6B92.2 (2)
H11F—C11B—H11G107.4Mo4B—O82B—Mo6B163.2 (2)
C11B—C12B—H12F109.5Mo7B—O82B—Mo6B96.67 (18)
C11B—C12B—H12H109.5Mo8B—O82B—Mo5B164.2 (2)
H12F—C12B—H12H109.5Mo4B—O82B—Mo5B85.87 (17)
C11B—C12B—H12G109.5Mo7B—O82B—Mo5B91.23 (17)
H12F—C12B—H12G109.5Mo6B—O82B—Mo5B84.84 (15)
H12H—C12B—H12G109.5Mo7B—O74B—Mo5B117.8 (2)
N1B—C17B—C18B117.4 (8)Mo7A—O73A—Mo3A110.3 (2)
N1B—C17B—H17G108.0Mo7A—O73A—Mo4A110.8 (2)
C18B—C17B—H17G108.0Mo3A—O73A—Mo4A104.0 (2)
N1B—C17B—H17F108.0Mo7B—O72B—Mo1B92.30 (18)
C18B—C17B—H17F108.0Mo7B—O72B—Mo8B103.61 (17)
H17G—C17B—H17F107.2Mo1B—O72B—Mo8B97.42 (18)
C17B—C18B—H18H109.5Mo7B—O72B—Mo3B91.93 (19)
C17B—C18B—H18F109.5Mo1B—O72B—Mo3B164.1 (2)
H18H—C18B—H18F109.5Mo8B—O72B—Mo3B96.50 (17)
C17B—C18B—H18G109.5Mo7B—O72B—Mo2B164.5 (2)
H18H—C18B—H18G109.5Mo1B—O72B—Mo2B86.48 (17)
H18F—C18B—H18G109.5Mo8B—O72B—Mo2B91.86 (16)
C14B—C13B—N1B116.7 (9)Mo3B—O72B—Mo2B85.35 (15)
C14B—C13B—H13G108.1Mo7B—O73B—Mo3B110.3 (2)
N1B—C13B—H13G108.1Mo7B—O73B—Mo4B110.6 (2)
C14B—C13B—H13F108.1Mo3B—O73B—Mo4B103.31 (19)
N1B—C13B—H13F108.1Mo8A—O84A—Mo2A119.6 (2)
H13G—C13B—H13F107.3Mo1A—O13A—Mo2A118.4 (3)
C13B—C14B—H14H109.5Mo4A—O43A—Mo5A117.6 (3)
C13B—C14B—H14F109.5Mo3A—O23A—Mo2A117.5 (3)
H14H—C14B—H14F109.5Mo6A—O53A—Mo5A117.8 (2)
C13B—C14B—H14G109.5Mo7A—O74A—Mo5A118.3 (2)
H14H—C14B—H14G109.5Mo3B—O23B—Mo2B118.0 (3)
H14F—C14B—H14G109.5Mo6B—O53B—Mo5B117.8 (3)
C16B—C15B—N1B118.1 (8)Mo1B—O13B—Mo2B117.7 (3)
C16B—C15B—H15F107.8Mo4B—O43B—Mo5B117.4 (3)
N1B—C15B—H15F107.8O81B—Mo8B—O84B104.9 (2)
C16B—C15B—H15G107.8O81B—Mo8B—O33B101.1 (2)
N1B—C15B—H15G107.8O84B—Mo8B—O33B96.0 (2)
H15F—C15B—H15G107.1O81B—Mo8B—O83B100.7 (2)
C15B—C16B—H16F109.5O84B—Mo8B—O83B96.4 (2)
C15B—C16B—H16H109.5O33B—Mo8B—O83B151.2 (2)
H16F—C16B—H16H109.5O81B—Mo8B—O82B99.2 (2)
C15B—C16B—H16G109.5O84B—Mo8B—O82B155.90 (19)
H16F—C16B—H16G109.5O33B—Mo8B—O82B78.9 (2)
H16H—C16B—H16G109.5O83B—Mo8B—O82B79.2 (2)
C38A—C37A—N3A115.5 (7)O81B—Mo8B—O72B175.1 (2)
C38A—C37A—H37C108.4O84B—Mo8B—O72B79.96 (19)
N3A—C37A—H37C108.4O33B—Mo8B—O72B78.62 (19)
C38A—C37A—H37D108.4O83B—Mo8B—O72B78.13 (18)
N3A—C37A—H37D108.4O82B—Mo8B—O72B75.94 (17)
H37C—C37A—H37D107.5O61B—Mo6B—O62B104.9 (3)
C37A—C38A—H38C109.5O61B—Mo6B—O53B102.8 (2)
C37A—C38A—H38D109.5O62B—Mo6B—O53B100.6 (3)
H38C—C38A—H38D109.5O61B—Mo6B—O83B101.2 (2)
C37A—C38A—H38E109.5O62B—Mo6B—O83B96.8 (2)
H38C—C38A—H38E109.5O53B—Mo6B—O83B145.5 (2)
H38D—C38A—H38E109.5O61B—Mo6B—O63B90.6 (2)
C34A—C33A—N3A115.5 (8)O62B—Mo6B—O63B162.4 (2)
C34A—C33A—H33C108.4O53B—Mo6B—O63B83.6 (2)
N3A—C33A—H33C108.4O83B—Mo6B—O63B71.70 (18)
C34A—C33A—H33D108.4O61B—Mo6B—O82B161.2 (2)
N3A—C33A—H33D108.4O62B—Mo6B—O82B93.4 (2)
H33C—C33A—H33D107.5O53B—Mo6B—O82B77.33 (19)
C33A—C34A—H34E109.5O83B—Mo6B—O82B72.02 (19)
C33A—C34A—H34D109.5O63B—Mo6B—O82B70.63 (16)
H34E—C34A—H34D109.5O81A—Mo8A—O84A104.8 (2)
C33A—C34A—H34C109.5O81A—Mo8A—O33A101.1 (2)
H34E—C34A—H34C109.5O84A—Mo8A—O33A96.5 (2)
H34D—C34A—H34C109.5O81A—Mo8A—O83A101.3 (2)
C32A—C31A—N3A114.1 (8)O84A—Mo8A—O83A96.2 (2)
C32A—C31A—H31C108.7O33A—Mo8A—O83A150.4 (2)
N3A—C31A—H31C108.7O81A—Mo8A—O82A99.6 (2)
C32A—C31A—H31D108.7O84A—Mo8A—O82A155.6 (2)
N3A—C31A—H31D108.7O33A—Mo8A—O82A78.7 (2)
H31C—C31A—H31D107.6O83A—Mo8A—O82A78.7 (2)
C31A—C32A—H32C109.5O81A—Mo8A—O72A175.1 (2)
C31A—C32A—H32D109.5O84A—Mo8A—O72A80.1 (2)
H32C—C32A—H32D109.5O33A—Mo8A—O72A78.68 (19)
C31A—C32A—H32E109.5O83A—Mo8A—O72A77.38 (18)
H32C—C32A—H32E109.5O82A—Mo8A—O72A75.50 (17)
H32D—C32A—H32E109.5O71A—Mo7A—O74A103.9 (2)
N3A—C35A—C36A115.2 (8)O71A—Mo7A—O63A101.5 (2)
N3A—C35A—H35C108.5O74A—Mo7A—O63A96.8 (2)
C36A—C35A—H35C108.5O71A—Mo7A—O73A101.5 (2)
N3A—C35A—H35D108.5O74A—Mo7A—O73A96.7 (2)
C36A—C35A—H35D108.5O63A—Mo7A—O73A149.6 (2)
H35C—C35A—H35D107.5O71A—Mo7A—O72A99.4 (2)
C35A—C36A—H36D109.5O74A—Mo7A—O72A156.68 (18)
C35A—C36A—H36E109.5O63A—Mo7A—O72A78.36 (19)
H36D—C36A—H36E109.5O73A—Mo7A—O72A78.47 (19)
C35A—C36A—H36C109.5O71A—Mo7A—O82A174.9 (2)
H36D—C36A—H36C109.5O74A—Mo7A—O82A81.16 (19)
H36E—C36A—H36C109.5O63A—Mo7A—O82A77.95 (19)
C32B—C31B—N3B115.2 (10)O73A—Mo7A—O82A77.35 (19)
C32B—C31B—H31F108.5O72A—Mo7A—O82A75.52 (16)
N3B—C31B—H31F108.5O71B—Mo7B—O74B103.5 (2)
C32B—C31B—H31G108.5O71B—Mo7B—O63B102.2 (2)
N3B—C31B—H31G108.5O74B—Mo7B—O63B96.2 (2)
H31F—C31B—H31G107.5O71B—Mo7B—O73B100.7 (2)
C31B—C32B—H32F109.5O74B—Mo7B—O73B96.2 (2)
C31B—C32B—H32G109.5O63B—Mo7B—O73B150.6 (2)
H32F—C32B—H32G109.5O71B—Mo7B—O72B99.7 (2)
C31B—C32B—H32H109.5O74B—Mo7B—O72B156.80 (18)
H32F—C32B—H32H109.5O63B—Mo7B—O72B78.9 (2)
H32G—C32B—H32H109.5O73B—Mo7B—O72B79.3 (2)
C35B—C36B—H36G109.5O71B—Mo7B—O82B175.5 (2)
C35B—C36B—H36H109.5O74B—Mo7B—O82B80.90 (19)
H36G—C36B—H36H109.5O63B—Mo7B—O82B78.08 (19)
C35B—C36B—H36F109.5O73B—Mo7B—O82B77.73 (19)
H36G—C36B—H36F109.5O72B—Mo7B—O82B75.89 (16)
H36H—C36B—H36F109.5O52B—Mo5B—O51B104.8 (3)
C36B—C35B—N3B118.3 (10)O52B—Mo5B—O53B104.0 (2)
C36B—C35B—H35F107.7O51B—Mo5B—O53B97.6 (3)
N3B—C35B—H35F107.7O52B—Mo5B—O43B101.5 (2)
C36B—C35B—H35G107.7O51B—Mo5B—O43B97.2 (2)
N3B—C35B—H35G107.7O53B—Mo5B—O43B145.9 (2)
H35F—C35B—H35G107.1O52B—Mo5B—O74B92.9 (2)
C34B—C33B—N3B115.5 (10)O51B—Mo5B—O74B162.2 (2)
C34B—C33B—H33F108.4O53B—Mo5B—O74B78.6 (2)
N3B—C33B—H33F108.4O43B—Mo5B—O74B77.98 (19)
C34B—C33B—H33G108.4O52B—Mo5B—O82B162.9 (2)
N3B—C33B—H33G108.4O51B—Mo5B—O82B92.1 (2)
H33F—C33B—H33G107.5O53B—Mo5B—O82B75.04 (19)
C33B—C34B—H34H109.5O43B—Mo5B—O82B73.9 (2)
C33B—C34B—H34G109.5O74B—Mo5B—O82B70.10 (17)
H34H—C34B—H34G109.5O31A—Mo3A—O32A104.3 (3)
C33B—C34B—H34F109.5O31A—Mo3A—O23A102.5 (2)
H34H—C34B—H34F109.5O32A—Mo3A—O23A100.7 (2)
H34G—C34B—H34F109.5O31A—Mo3A—O73A100.6 (2)
C37B—C38B—H38F109.5O32A—Mo3A—O73A97.3 (2)
C37B—C38B—H38G109.5O23A—Mo3A—O73A145.9 (2)
H38F—C38B—H38G109.5O31A—Mo3A—O33A90.2 (2)
C37B—C38B—H38H109.5O32A—Mo3A—O33A163.3 (2)
H38F—C38B—H38H109.5O23A—Mo3A—O33A83.7 (2)
H38G—C38B—H38H109.5O73A—Mo3A—O33A71.56 (18)
N3B—C37B—C38B115.6 (9)O31A—Mo3A—O72A162.0 (2)
N3B—C37B—H37G108.4O32A—Mo3A—O72A93.2 (2)
C38B—C37B—H37G108.4O23A—Mo3A—O72A77.9 (2)
N3B—C37B—H37F108.4O73A—Mo3A—O72A72.48 (19)
C38B—C37B—H37F108.4O33A—Mo3A—O72A71.89 (15)
H37G—C37B—H37F107.4O31B—Mo3B—O32B104.8 (3)
C25B—C26B—H26H109.5O31B—Mo3B—O23B103.6 (2)
C25B—C26B—H26F109.5O32B—Mo3B—O23B100.6 (2)
H26H—C26B—H26F109.5O31B—Mo3B—O73B101.1 (2)
C25B—C26B—H26G109.5O32B—Mo3B—O73B96.8 (2)
H26H—C26B—H26G109.5O23B—Mo3B—O73B144.9 (2)
H26F—C26B—H26G109.5O31B—Mo3B—O33B89.9 (2)
C26B—C25B—N2B116.5 (7)O32B—Mo3B—O33B163.0 (2)
C26B—C25B—H25G108.2O23B—Mo3B—O33B83.64 (19)
N2B—C25B—H25G108.2O73B—Mo3B—O33B71.68 (17)
C26B—C25B—H25F108.2O31B—Mo3B—O72B161.2 (2)
N2B—C25B—H25F108.2O32B—Mo3B—O72B93.6 (2)
H25G—C25B—H25F107.3O23B—Mo3B—O72B76.43 (19)
N2B—C27B—C28B115.2 (7)O73B—Mo3B—O72B72.24 (18)
N2B—C27B—H27F108.5O33B—Mo3B—O72B71.28 (16)
C28B—C27B—H27F108.5O22A—Mo2A—O21A104.5 (3)
N2B—C27B—H27G108.5O22A—Mo2A—O23A103.8 (2)
C28B—C27B—H27G108.5O21A—Mo2A—O23A97.7 (2)
H27F—C27B—H27G107.5O22A—Mo2A—O13A102.7 (2)
C27B—C28B—H28G109.5O21A—Mo2A—O13A97.6 (2)
C27B—C28B—H28F109.5O23A—Mo2A—O13A144.8 (2)
H28G—C28B—H28F109.5O22A—Mo2A—O84A93.3 (2)
C27B—C28B—H28H109.5O21A—Mo2A—O84A162.3 (2)
H28G—C28B—H28H109.5O23A—Mo2A—O84A77.75 (19)
H28F—C28B—H28H109.5O13A—Mo2A—O84A78.04 (18)
N2B—C21B—C22B113.5 (7)O22A—Mo2A—O72A162.5 (2)
N2B—C21B—H21F108.9O21A—Mo2A—O72A93.0 (2)
C22B—C21B—H21F108.9O23A—Mo2A—O72A74.42 (19)
N2B—C21B—H21G108.9O13A—Mo2A—O72A73.28 (19)
C22B—C21B—H21G108.9O84A—Mo2A—O72A69.23 (16)
H21F—C21B—H21G107.7O22B—Mo2B—O21B104.4 (3)
C21B—C22B—H22G109.5O22B—Mo2B—O23B104.5 (2)
C21B—C22B—H22H109.5O21B—Mo2B—O23B97.4 (2)
H22G—C22B—H22H109.5O22B—Mo2B—O13B101.1 (2)
C21B—C22B—H22F109.5O21B—Mo2B—O13B97.3 (2)
H22G—C22B—H22F109.5O23B—Mo2B—O13B146.1 (2)
H22H—C22B—H22F109.5O22B—Mo2B—O84B93.8 (2)
C24B—C23B—N2B115.6 (7)O21B—Mo2B—O84B161.8 (2)
C24B—C23B—H23F108.4O23B—Mo2B—O84B78.25 (19)
N2B—C23B—H23F108.4O13B—Mo2B—O84B78.25 (19)
C24B—C23B—H23G108.4O22B—Mo2B—O72B163.6 (2)
N2B—C23B—H23G108.4O21B—Mo2B—O72B91.9 (2)
H23F—C23B—H23G107.4O23B—Mo2B—O72B75.19 (19)
N2A—C25A—C26A113.0 (7)O13B—Mo2B—O72B73.91 (19)
N2A—C25A—H25D109.0O84B—Mo2B—O72B69.90 (17)
C26A—C25A—H25D109.0O61A—Mo6A—O62A104.8 (3)
N2A—C25A—H25C109.0O61A—Mo6A—O53A102.6 (2)
C26A—C25A—H25C109.0O62A—Mo6A—O53A101.3 (2)
H25D—C25A—H25C107.8O61A—Mo6A—O83A100.5 (2)
C25A—C26A—H26E109.5O62A—Mo6A—O83A95.9 (2)
C25A—C26A—H26D109.5O53A—Mo6A—O83A146.5 (2)
H26E—C26A—H26D109.5O61A—Mo6A—O63A89.9 (2)
C25A—C26A—H26C109.5O62A—Mo6A—O63A162.5 (2)
H26E—C26A—H26C109.5O53A—Mo6A—O63A84.21 (19)
H26D—C26A—H26C109.5O83A—Mo6A—O63A71.80 (17)
N2A—C27A—C28A113.9 (7)O61A—Mo6A—O82A161.3 (2)
N2A—C27A—H27D108.8O62A—Mo6A—O82A93.3 (2)
C28A—C27A—H27D108.8O53A—Mo6A—O82A77.9 (2)
N2A—C27A—H27C108.8O83A—Mo6A—O82A72.50 (19)
C28A—C27A—H27C108.8O63A—Mo6A—O82A71.48 (16)
H27D—C27A—H27C107.7O41A—Mo4A—O42A105.2 (3)
C27A—C28A—H28D109.5O41A—Mo4A—O43A101.5 (2)
C27A—C28A—H28E109.5O42A—Mo4A—O43A100.9 (2)
H28D—C28A—H28E109.5O41A—Mo4A—O33A100.8 (2)
C27A—C28A—H28C109.5O42A—Mo4A—O33A95.7 (2)
H28D—C28A—H28C109.5O43A—Mo4A—O33A147.6 (2)
H28E—C28A—H28C109.5O41A—Mo4A—O73A89.0 (2)
C22A—C21A—N2A115.3 (7)O42A—Mo4A—O73A162.9 (2)
C22A—C21A—H21C108.5O43A—Mo4A—O73A85.17 (18)
N2A—C21A—H21C108.5O33A—Mo4A—O73A71.93 (18)
C22A—C21A—H21D108.5O41A—Mo4A—O82A160.3 (2)
N2A—C21A—H21D108.5O42A—Mo4A—O82A94.1 (2)
H21C—C21A—H21D107.5O43A—Mo4A—O82A78.2 (2)
C21A—C22A—H22D109.5O33A—Mo4A—O82A72.90 (19)
C21A—C22A—H22C109.5O73A—Mo4A—O82A71.28 (17)
H22D—C22A—H22C109.5O52A—Mo5A—O51A103.6 (3)
C21A—C22A—H22E109.5O52A—Mo5A—O53A104.0 (2)
H22D—C22A—H22E109.5O51A—Mo5A—O53A98.3 (3)
H22C—C22A—H22E109.5O52A—Mo5A—O43A102.3 (3)
N2A—C23A—C24A116.1 (7)O51A—Mo5A—O43A97.8 (2)
N2A—C23A—H23C108.3O53A—Mo5A—O43A144.8 (2)
C24A—C23A—H23C108.3O52A—Mo5A—O74A93.7 (2)
N2A—C23A—H23D108.3O51A—Mo5A—O74A162.7 (2)
C24A—C23A—H23D108.3O53A—Mo5A—O74A77.6 (2)
H23C—C23A—H23D107.4O43A—Mo5A—O74A77.75 (19)
C16A—C15A—N1A117.9 (9)O52A—Mo5A—O82A162.9 (2)
C16A—C15A—H15C107.8O51A—Mo5A—O82A93.5 (2)
N1A—C15A—H15C107.8O53A—Mo5A—O82A74.16 (19)
C16A—C15A—H15D107.8O43A—Mo5A—O82A73.80 (19)
N1A—C15A—H15D107.8O74A—Mo5A—O82A69.19 (17)
H15C—C15A—H15D107.2O41B—Mo4B—O42B105.0 (3)
C15A—C16A—H16C109.5O41B—Mo4B—O43B101.6 (2)
C15A—C16A—H16E109.5O42B—Mo4B—O43B101.9 (2)
H16C—C16A—H16E109.5O41B—Mo4B—O33B100.9 (2)
C15A—C16A—H16D109.5O42B—Mo4B—O33B96.2 (2)
H16C—C16A—H16D109.5O43B—Mo4B—O33B146.3 (2)
H16E—C16A—H16D109.5O41B—Mo4B—O73B88.6 (2)
C12A—C11A—N1A116.7 (9)O42B—Mo4B—O73B163.6 (2)
C12A—C11A—H11C108.1O43B—Mo4B—O73B83.92 (18)
N1A—C11A—H11C108.1O33B—Mo4B—O73B71.83 (18)
C12A—C11A—H11D108.1O41B—Mo4B—O82B159.8 (2)
N1A—C11A—H11D108.1O42B—Mo4B—O82B94.8 (2)
H11C—C11A—H11D107.3O43B—Mo4B—O82B77.8 (2)
C11A—C12A—H12C109.5O33B—Mo4B—O82B72.50 (19)
C11A—C12A—H12E109.5O73B—Mo4B—O82B71.24 (17)
H12C—C12A—H12E109.5O11A—Mo1A—O12A104.1 (3)
C11A—C12A—H12D109.5O11A—Mo1A—O13A101.9 (2)
H12C—C12A—H12D109.5O12A—Mo1A—O13A100.9 (2)
H12E—C12A—H12D109.5O11A—Mo1A—O63A100.7 (2)
N1A—C13A—C14A116.4 (10)O12A—Mo1A—O63A96.3 (2)
N1A—C13A—H13D108.2O13A—Mo1A—O63A147.19 (19)
C14A—C13A—H13D108.2O11A—Mo1A—O83A88.9 (2)
N1A—C13A—H13C108.2O12A—Mo1A—O83A164.0 (2)
C14A—C13A—H13C108.2O13A—Mo1A—O83A85.05 (17)
H13D—C13A—H13C107.3O63A—Mo1A—O83A71.83 (18)
C13A—C14A—H14E109.5O11A—Mo1A—O72A160.9 (2)
C13A—C14A—H14C109.5O12A—Mo1A—O72A94.6 (2)
H14E—C14A—H14C109.5O13A—Mo1A—O72A77.85 (19)
C13A—C14A—H14D109.5O63A—Mo1A—O72A73.11 (18)
H14E—C14A—H14D109.5O83A—Mo1A—O72A72.01 (16)
H14C—C14A—H14D109.5O11B—Mo1B—O12B104.1 (3)
N1A—C17A—C18A115.2 (12)O11B—Mo1B—O13B101.7 (2)
N1A—C17A—H17D108.5O12B—Mo1B—O13B101.7 (2)
C18A—C17A—H17D108.5O11B—Mo1B—O63B101.6 (2)
N1A—C17A—H17C108.5O12B—Mo1B—O63B96.7 (2)
C18A—C17A—H17C108.5O13B—Mo1B—O63B145.7 (2)
H17D—C17A—H17C107.5O11B—Mo1B—O72B161.0 (2)
C17A—C18A—H18E109.5O12B—Mo1B—O72B94.7 (2)
C17A—C18A—H18C109.5O13B—Mo1B—O72B77.12 (19)
H18E—C18A—H18C109.5O63B—Mo1B—O72B72.69 (18)
C17A—C18A—H18D109.5O11B—Mo1B—O83B89.3 (2)
H18E—C18A—H18D109.5O12B—Mo1B—O83B163.6 (2)
H18C—C18A—H18D109.5O13B—Mo1B—O83B84.36 (19)
C23B—C24B—H24F109.5O63B—Mo1B—O83B71.08 (19)
C23B—C24B—H24H109.5O72B—Mo1B—O83B71.64 (16)
H24F—C24B—H24H109.5C17B—N1B—C15B111.4 (8)
C23B—C24B—H24G109.5C17B—N1B—C11B104.8 (7)
H24F—C24B—H24G109.5C15B—N1B—C11B111.5 (8)
H24H—C24B—H24G109.5C17B—N1B—C13B111.5 (7)
C23A—C24A—H24C109.5C15B—N1B—C13B106.3 (7)
C23A—C24A—H24D109.5C11B—N1B—C13B111.5 (8)
H24C—C24A—H24D109.5C35A—N3A—C37A112.5 (7)
C23A—C24A—H24E109.5C35A—N3A—C33A105.0 (7)
H24C—C24A—H24E109.5C37A—N3A—C33A111.3 (7)
H24D—C24A—H24E109.5C35A—N3A—C31A110.1 (7)
Mo7A—O63A—Mo1A109.4 (2)C37A—N3A—C31A106.3 (6)
Mo7A—O63A—Mo6A110.9 (2)C33A—N3A—C31A111.8 (8)
Mo1A—O63A—Mo6A103.5 (2)C37B—N3B—C33B110.7 (8)
Mo7B—O63B—Mo1B109.4 (2)C37B—N3B—C35B111.9 (9)
Mo7B—O63B—Mo6B111.7 (2)C33B—N3B—C35B106.5 (8)
Mo1B—O63B—Mo6B103.7 (2)C37B—N3B—C31B103.9 (7)
Mo8A—O33A—Mo4A109.4 (2)C33B—N3B—C31B113.4 (8)
Mo8A—O33A—Mo3A110.1 (2)C35B—N3B—C31B110.4 (9)
Mo4A—O33A—Mo3A103.0 (2)C21B—N2B—C27B113.1 (7)
Mo8B—O84B—Mo2B118.3 (2)C21B—N2B—C23B105.9 (6)
Mo8B—O33B—Mo4B109.3 (2)C27B—N2B—C23B111.8 (7)
Mo8B—O33B—Mo3B111.0 (2)C21B—N2B—C25B109.5 (6)
Mo4B—O33B—Mo3B102.9 (2)C27B—N2B—C25B106.6 (6)
Mo8A—O82A—Mo4A92.75 (19)C23B—N2B—C25B109.9 (7)
Mo8A—O82A—Mo6A92.6 (2)C27A—N2A—C21A112.8 (7)
Mo4A—O82A—Mo6A163.4 (2)C27A—N2A—C23A110.4 (6)
Mo8A—O82A—Mo7A104.85 (18)C21A—N2A—C23A105.5 (6)
Mo4A—O82A—Mo7A97.27 (19)C27A—N2A—C25A106.0 (6)
Mo6A—O82A—Mo7A96.56 (18)C21A—N2A—C25A110.9 (7)
Mo8A—O82A—Mo5A163.8 (2)C23A—N2A—C25A111.4 (7)
Mo4A—O82A—Mo5A85.64 (17)C17A—N1A—C15A111.1 (9)
Mo6A—O82A—Mo5A84.87 (16)C17A—N1A—C13A114.9 (9)
Mo7A—O82A—Mo5A91.37 (18)C15A—N1A—C13A104.8 (8)
Mo8A—O83A—Mo6A109.7 (2)C17A—N1A—C11A104.3 (9)
Mo8A—O83A—Mo1A110.5 (2)C15A—N1A—C11A111.2 (9)
Mo6A—O83A—Mo1A103.5 (2)C13A—N1A—C11A110.7 (9)
Mo8B—O83B—Mo6B110.2 (2)H1N—N4A—H2N112
Mo8B—O83B—Mo1B110.1 (2)H1N—N4A—H3N100
Mo6B—O83B—Mo1B103.3 (2)H2N—N4A—H3N104
Mo7A—O72A—Mo1A92.79 (17)H1N—N4A—H4N117
Mo7A—O72A—Mo3A92.2 (2)H2N—N4A—H4N116
Mo1A—O72A—Mo3A163.9 (2)H3N—N4A—H4N106
Mo7A—O72A—Mo8A104.12 (18)H5N—N4B—H6N105
Mo1A—O72A—Mo8A97.16 (18)H5N—N4B—H7N117
Mo3A—O72A—Mo8A96.48 (17)H6N—N4B—H7N102
Mo7A—O72A—Mo2A164.9 (2)H5N—N4B—H8N101
Mo1A—O72A—Mo2A86.17 (17)H6N—N4B—H8N117
Mo3A—O72A—Mo2A85.00 (15)H7N—N4B—H8N115
Mo2B—O84B—Mo8B—O81B−179.8 (3)Mo8B—O72B—Mo3B—O32B177.3 (2)
Mo2B—O84B—Mo8B—O33B−76.7 (3)Mo2B—O72B—Mo3B—O32B85.9 (2)
Mo2B—O84B—Mo8B—O83B77.3 (3)Mo7B—O72B—Mo3B—O23B−178.8 (2)
Mo2B—O84B—Mo8B—O82B−0.6 (7)Mo1B—O72B—Mo3B—O23B−73.5 (9)
Mo2B—O84B—Mo8B—O72B0.6 (2)Mo8B—O72B—Mo3B—O23B77.2 (2)
Mo4B—O33B—Mo8B—O81B−75.5 (3)Mo2B—O72B—Mo3B—O23B−14.12 (17)
Mo3B—O33B—Mo8B—O81B171.6 (2)Mo7B—O72B—Mo3B—O73B17.25 (16)
Mo4B—O33B—Mo8B—O84B178.0 (2)Mo1B—O72B—Mo3B—O73B122.6 (9)
Mo3B—O33B—Mo8B—O84B65.1 (2)Mo8B—O72B—Mo3B—O73B−86.68 (18)
Mo4B—O33B—Mo8B—O83B62.8 (5)Mo2B—O72B—Mo3B—O73B−178.03 (19)
Mo3B—O33B—Mo8B—O83B−50.0 (5)Mo7B—O72B—Mo3B—O33B93.37 (17)
Mo4B—O33B—Mo8B—O82B21.8 (2)Mo1B—O72B—Mo3B—O33B−161.3 (9)
Mo3B—O33B—Mo8B—O82B−91.0 (2)Mo8B—O72B—Mo3B—O33B−10.57 (15)
Mo4B—O33B—Mo8B—O72B99.5 (2)Mo2B—O72B—Mo3B—O33B−101.92 (17)
Mo3B—O33B—Mo8B—O72B−13.32 (19)Mo3A—O23A—Mo2A—O22A177.8 (3)
Mo6B—O83B—Mo8B—O81B75.3 (3)Mo3A—O23A—Mo2A—O21A70.7 (3)
Mo1B—O83B—Mo8B—O81B−171.5 (2)Mo3A—O23A—Mo2A—O13A−44.3 (5)
Mo6B—O83B—Mo8B—O84B−178.2 (2)Mo3A—O23A—Mo2A—O84A−91.8 (3)
Mo1B—O83B—Mo8B—O84B−64.9 (3)Mo3A—O23A—Mo2A—O72A−20.3 (2)
Mo6B—O83B—Mo8B—O33B−63.2 (5)Mo1A—O13A—Mo2A—O22A−179.1 (3)
Mo1B—O83B—Mo8B—O33B50.1 (5)Mo1A—O13A—Mo2A—O21A−72.3 (3)
Mo6B—O83B—Mo8B—O82B−22.2 (2)Mo1A—O13A—Mo2A—O23A42.8 (5)
Mo1B—O83B—Mo8B—O82B91.1 (2)Mo1A—O13A—Mo2A—O84A90.2 (3)
Mo6B—O83B—Mo8B—O72B−99.9 (2)Mo1A—O13A—Mo2A—O72A18.6 (2)
Mo1B—O83B—Mo8B—O72B13.35 (19)Mo8A—O84A—Mo2A—O22A−179.7 (3)
Mo4B—O82B—Mo8B—O81B82.0 (2)Mo8A—O84A—Mo2A—O21A0.1 (9)
Mo7B—O82B—Mo8B—O81B−179.4 (2)Mo8A—O84A—Mo2A—O23A76.9 (3)
Mo6B—O82B—Mo8B—O81B−82.0 (2)Mo8A—O84A—Mo2A—O13A−77.3 (3)
Mo5B—O82B—Mo8B—O81B−3.3 (10)Mo8A—O84A—Mo2A—O72A−0.9 (2)
Mo4B—O82B—Mo8B—O84B−97.2 (5)Mo7A—O72A—Mo2A—O22A−179.0 (8)
Mo7B—O82B—Mo8B—O84B1.3 (6)Mo1A—O72A—Mo2A—O22A−92.5 (7)
Mo6B—O82B—Mo8B—O84B98.8 (5)Mo3A—O72A—Mo2A—O22A101.0 (7)
Mo5B—O82B—Mo8B—O84B177.5 (7)Mo8A—O72A—Mo2A—O22A4.6 (8)
Mo4B—O82B—Mo8B—O33B−17.54 (16)Mo7A—O72A—Mo2A—O21A−2.8 (10)
Mo7B—O82B—Mo8B—O33B81.0 (2)Mo1A—O72A—Mo2A—O21A83.7 (2)
Mo6B—O82B—Mo8B—O33B178.5 (2)Mo3A—O72A—Mo2A—O21A−82.7 (2)
Mo5B—O82B—Mo8B—O33B−102.8 (10)Mo8A—O72A—Mo2A—O21A−179.1 (2)
Mo4B—O82B—Mo8B—O83B−178.8 (2)Mo7A—O72A—Mo2A—O23A94.4 (9)
Mo7B—O82B—Mo8B—O83B−80.2 (2)Mo1A—O72A—Mo2A—O23A−179.1 (2)
Mo6B—O82B—Mo8B—O83B17.26 (16)Mo3A—O72A—Mo2A—O23A14.44 (18)
Mo5B—O82B—Mo8B—O83B95.9 (10)Mo8A—O72A—Mo2A—O23A−82.0 (2)
Mo4B—O82B—Mo8B—O72B−98.45 (16)Mo7A—O72A—Mo2A—O13A−99.8 (10)
Mo7B—O82B—Mo8B—O72B0.1 (2)Mo1A—O72A—Mo2A—O13A−13.29 (16)
Mo6B—O82B—Mo8B—O72B97.58 (15)Mo3A—O72A—Mo2A—O13A−179.8 (2)
Mo5B—O82B—Mo8B—O72B176.3 (9)Mo8A—O72A—Mo2A—O13A83.82 (19)
Mo7B—O72B—Mo8B—O81B5(3)Mo7A—O72A—Mo2A—O84A176.9 (10)
Mo1B—O72B—Mo8B—O81B−89 (3)Mo1A—O72A—Mo2A—O84A−96.54 (17)
Mo3B—O72B—Mo8B—O81B99 (3)Mo3A—O72A—Mo2A—O84A96.98 (17)
Mo2B—O72B—Mo8B—O81B−176 (3)Mo8A—O72A—Mo2A—O84A0.57 (15)
Mo7B—O72B—Mo8B—O84B−179.6 (3)Mo3B—O23B—Mo2B—O22B176.7 (3)
Mo1B—O72B—Mo8B—O84B86.2 (2)Mo3B—O23B—Mo2B—O21B69.7 (3)
Mo3B—O72B—Mo8B—O84B−86.0 (2)Mo3B—O23B—Mo2B—O13B−45.3 (5)
Mo2B—O72B—Mo8B—O84B−0.52 (19)Mo3B—O23B—Mo2B—O84B−92.3 (3)
Mo7B—O72B—Mo8B—O33B−81.4 (2)Mo3B—O23B—Mo2B—O72B−20.3 (2)
Mo1B—O72B—Mo8B—O33B−175.5 (2)Mo1B—O13B—Mo2B—O22B−176.6 (3)
Mo3B—O72B—Mo8B—O33B12.23 (18)Mo1B—O13B—Mo2B—O21B−70.3 (3)
Mo2B—O72B—Mo8B—O33B97.76 (19)Mo1B—O13B—Mo2B—O23B44.8 (5)
Mo7B—O72B—Mo8B—O83B81.6 (2)Mo1B—O13B—Mo2B—O84B91.8 (3)
Mo1B—O72B—Mo8B—O83B−12.64 (18)Mo1B—O13B—Mo2B—O72B19.6 (2)
Mo3B—O72B—Mo8B—O83B175.1 (2)Mo8B—O84B—Mo2B—O22B−178.2 (3)
Mo2B—O72B—Mo8B—O83B−99.3 (2)Mo8B—O84B—Mo2B—O21B−0.1 (8)
Mo7B—O72B—Mo8B—O82B−0.1 (3)Mo8B—O84B—Mo2B—O23B77.7 (3)
Mo1B—O72B—Mo8B—O82B−94.33 (19)Mo8B—O84B—Mo2B—O13B−77.6 (3)
Mo3B—O72B—Mo8B—O82B93.46 (17)Mo8B—O84B—Mo2B—O72B−0.6 (2)
Mo2B—O72B—Mo8B—O82B178.99 (13)Mo7B—O72B—Mo2B—O22B−174.2 (8)
Mo5B—O53B—Mo6B—O61B178.7 (3)Mo1B—O72B—Mo2B—O22B−88.3 (8)
Mo5B—O53B—Mo6B—O62B70.6 (3)Mo8B—O72B—Mo2B—O22B9.0 (8)
Mo5B—O53B—Mo6B—O83B−48.3 (5)Mo3B—O72B—Mo2B—O22B105.4 (7)
Mo5B—O53B—Mo6B—O63B−92.1 (3)Mo7B—O72B—Mo2B—O21B−2.6 (10)
Mo5B—O53B—Mo6B—O82B−20.6 (3)Mo1B—O72B—Mo2B—O21B83.3 (2)
Mo8B—O83B—Mo6B—O61B−178.0 (3)Mo8B—O72B—Mo2B—O21B−179.4 (2)
Mo1B—O83B—Mo6B—O61B64.4 (3)Mo3B—O72B—Mo2B—O21B−83.0 (2)
Mo8B—O83B—Mo6B—O62B−71.2 (3)Mo7B—O72B—Mo2B—O23B94.5 (10)
Mo1B—O83B—Mo6B—O62B171.2 (3)Mo1B—O72B—Mo2B—O23B−179.58 (19)
Mo8B—O83B—Mo6B—O53B48.7 (4)Mo8B—O72B—Mo2B—O23B−82.3 (2)
Mo1B—O83B—Mo6B—O53B−68.9 (4)Mo3B—O72B—Mo2B—O23B14.12 (18)
Mo8B—O83B—Mo6B—O63B95.1 (2)Mo7B—O72B—Mo2B—O13B−99.7 (10)
Mo1B—O83B—Mo6B—O63B−22.46 (16)Mo1B—O72B—Mo2B—O13B−13.80 (16)
Mo8B—O83B—Mo6B—O82B20.17 (19)Mo8B—O72B—Mo2B—O13B83.52 (19)
Mo1B—O83B—Mo6B—O82B−97.4 (2)Mo3B—O72B—Mo2B—O13B179.9 (2)
Mo7B—O63B—Mo6B—O61B167.3 (3)Mo7B—O72B—Mo2B—O84B177.2 (10)
Mo1B—O63B—Mo6B—O61B−75.0 (3)Mo1B—O72B—Mo2B—O84B−96.90 (18)
Mo7B—O63B—Mo6B—O62B−40.3 (9)Mo8B—O72B—Mo2B—O84B0.42 (15)
Mo1B—O63B—Mo6B—O62B77.4 (8)Mo3B—O72B—Mo2B—O84B96.79 (17)
Mo7B—O63B—Mo6B—O53B64.4 (2)Mo5A—O53A—Mo6A—O61A177.8 (3)
Mo1B—O63B—Mo6B—O53B−177.9 (2)Mo5A—O53A—Mo6A—O62A69.7 (3)
Mo7B—O63B—Mo6B—O83B−91.2 (3)Mo5A—O53A—Mo6A—O83A−49.7 (5)
Mo1B—O63B—Mo6B—O83B26.5 (2)Mo5A—O53A—Mo6A—O63A−93.6 (3)
Mo7B—O63B—Mo6B—O82B−14.4 (2)Mo5A—O53A—Mo6A—O82A−21.3 (3)
Mo1B—O63B—Mo6B—O82B103.3 (2)Mo8A—O83A—Mo6A—O61A−177.4 (3)
Mo8B—O82B—Mo6B—O61B−88.8 (7)Mo1A—O83A—Mo6A—O61A64.7 (3)
Mo4B—O82B—Mo6B—O61B163.6 (8)Mo8A—O83A—Mo6A—O62A−71.1 (3)
Mo7B—O82B—Mo6B—O61B16.2 (8)Mo1A—O83A—Mo6A—O62A171.0 (2)
Mo5B—O82B—Mo6B—O61B106.8 (7)Mo8A—O83A—Mo6A—O53A49.7 (4)
Mo8B—O82B—Mo6B—O62B78.5 (2)Mo1A—O83A—Mo6A—O53A−68.2 (4)
Mo4B—O82B—Mo6B—O62B−29.2 (9)Mo8A—O83A—Mo6A—O63A96.2 (2)
Mo7B—O82B—Mo6B—O62B−176.6 (2)Mo1A—O83A—Mo6A—O63A−21.72 (17)
Mo5B—O82B—Mo6B—O62B−85.9 (2)Mo8A—O83A—Mo6A—O82A20.49 (19)
Mo8B—O82B—Mo6B—O53B178.6 (2)Mo1A—O83A—Mo6A—O82A−97.4 (2)
Mo4B—O82B—Mo6B—O53B70.9 (9)Mo7A—O63A—Mo6A—O61A166.9 (3)
Mo7B—O82B—Mo6B—O53B−76.5 (2)Mo1A—O63A—Mo6A—O61A−75.9 (2)
Mo5B—O82B—Mo6B—O53B14.16 (18)Mo7A—O63A—Mo6A—O62A−45.3 (8)
Mo8B—O82B—Mo6B—O83B−17.50 (16)Mo1A—O63A—Mo6A—O62A71.9 (8)
Mo4B—O82B—Mo6B—O83B−125.2 (9)Mo7A—O63A—Mo6A—O53A64.2 (2)
Mo7B—O82B—Mo6B—O83B87.43 (18)Mo1A—O63A—Mo6A—O53A−178.6 (2)
Mo5B—O82B—Mo6B—O83B178.07 (19)Mo7A—O63A—Mo6A—O83A−92.0 (2)
Mo8B—O82B—Mo6B—O63B−93.86 (18)Mo1A—O63A—Mo6A—O83A25.1 (2)
Mo4B—O82B—Mo6B—O63B158.5 (9)Mo7A—O63A—Mo6A—O82A−14.9 (2)
Mo7B—O82B—Mo6B—O63B11.07 (16)Mo1A—O63A—Mo6A—O82A102.2 (2)
Mo5B—O82B—Mo6B—O63B101.71 (17)Mo8A—O82A—Mo6A—O61A−87.8 (7)
Mo2A—O84A—Mo8A—O81A−179.7 (3)Mo4A—O82A—Mo6A—O61A163.6 (8)
Mo2A—O84A—Mo8A—O33A−76.4 (3)Mo7A—O82A—Mo6A—O61A17.4 (8)
Mo2A—O84A—Mo8A—O83A76.9 (3)Mo5A—O82A—Mo6A—O61A108.2 (7)
Mo2A—O84A—Mo8A—O82A0.5 (7)Mo8A—O82A—Mo6A—O62A77.6 (2)
Mo2A—O84A—Mo8A—O72A0.9 (2)Mo4A—O82A—Mo6A—O62A−31.0 (9)
Mo4A—O33A—Mo8A—O81A−76.3 (3)Mo7A—O82A—Mo6A—O62A−177.2 (2)
Mo3A—O33A—Mo8A—O81A171.2 (2)Mo5A—O82A—Mo6A—O62A−86.4 (2)
Mo4A—O33A—Mo8A—O84A177.2 (2)Mo8A—O82A—Mo6A—O53A178.4 (2)
Mo3A—O33A—Mo8A—O84A64.7 (2)Mo4A—O82A—Mo6A—O53A69.9 (9)
Mo4A—O33A—Mo8A—O83A62.3 (5)Mo7A—O82A—Mo6A—O53A−76.3 (2)
Mo3A—O33A—Mo8A—O83A−50.2 (5)Mo5A—O82A—Mo6A—O53A14.48 (18)
Mo4A—O33A—Mo8A—O82A21.4 (2)Mo8A—O82A—Mo6A—O83A−17.58 (16)
Mo3A—O33A—Mo8A—O82A−91.1 (2)Mo4A—O82A—Mo6A—O83A−126.1 (9)
Mo4A—O33A—Mo8A—O72A98.7 (2)Mo7A—O82A—Mo6A—O83A87.69 (19)
Mo3A—O33A—Mo8A—O72A−13.83 (19)Mo5A—O82A—Mo6A—O83A178.5 (2)
Mo6A—O83A—Mo8A—O81A75.6 (3)Mo8A—O82A—Mo6A—O63A−93.71 (18)
Mo1A—O83A—Mo8A—O81A−170.9 (2)Mo4A—O82A—Mo6A—O63A157.7 (9)
Mo6A—O83A—Mo8A—O84A−177.9 (2)Mo7A—O82A—Mo6A—O63A11.56 (16)
Mo1A—O83A—Mo8A—O84A−64.5 (3)Mo5A—O82A—Mo6A—O63A102.35 (17)
Mo6A—O83A—Mo8A—O33A−62.9 (4)Mo5A—O43A—Mo4A—O41A−179.8 (3)
Mo1A—O83A—Mo8A—O33A50.5 (5)Mo5A—O43A—Mo4A—O42A−71.6 (3)
Mo6A—O83A—Mo8A—O82A−22.0 (2)Mo5A—O43A—Mo4A—O33A47.7 (5)
Mo1A—O83A—Mo8A—O82A91.4 (2)Mo5A—O43A—Mo4A—O73A92.2 (3)
Mo6A—O83A—Mo8A—O72A−99.5 (2)Mo5A—O43A—Mo4A—O82A20.3 (2)
Mo1A—O83A—Mo8A—O72A13.94 (19)Mo8A—O33A—Mo4A—O41A179.1 (3)
Mo4A—O82A—Mo8A—O81A82.2 (2)Mo3A—O33A—Mo4A—O41A−63.8 (2)
Mo6A—O82A—Mo8A—O81A−82.1 (2)Mo8A—O33A—Mo4A—O42A72.5 (3)
Mo7A—O82A—Mo8A—O81A−179.6 (2)Mo3A—O33A—Mo4A—O42A−170.5 (2)
Mo5A—O82A—Mo8A—O81A−1.7 (10)Mo8A—O33A—Mo4A—O43A−48.2 (5)
Mo4A—O82A—Mo8A—O84A−98.1 (5)Mo3A—O33A—Mo4A—O43A68.9 (4)
Mo6A—O82A—Mo8A—O84A97.7 (5)Mo8A—O33A—Mo4A—O73A−95.4 (2)
Mo7A—O82A—Mo8A—O84A0.2 (6)Mo3A—O33A—Mo4A—O73A21.62 (17)
Mo5A—O82A—Mo8A—O84A178.1 (7)Mo8A—O33A—Mo4A—O82A−20.08 (19)
Mo4A—O82A—Mo8A—O33A−17.34 (17)Mo3A—O33A—Mo4A—O82A97.0 (2)
Mo6A—O82A—Mo8A—O33A178.4 (2)Mo7A—O73A—Mo4A—O41A−165.4 (3)
Mo7A—O82A—Mo8A—O33A80.9 (2)Mo3A—O73A—Mo4A—O41A76.1 (3)
Mo5A—O82A—Mo8A—O33A−101.2 (9)Mo7A—O73A—Mo4A—O42A47.9 (8)
Mo4A—O82A—Mo8A—O83A−178.1 (2)Mo3A—O73A—Mo4A—O42A−70.6 (8)
Mo6A—O82A—Mo8A—O83A17.63 (16)Mo7A—O73A—Mo4A—O43A−63.8 (3)
Mo7A—O82A—Mo8A—O83A−79.9 (2)Mo3A—O73A—Mo4A—O43A177.7 (2)
Mo5A—O82A—Mo8A—O83A98.0 (10)Mo7A—O73A—Mo4A—O33A92.9 (3)
Mo4A—O82A—Mo8A—O72A−98.41 (16)Mo3A—O73A—Mo4A—O33A−25.5 (2)
Mo6A—O82A—Mo8A—O72A97.33 (15)Mo7A—O73A—Mo4A—O82A15.4 (2)
Mo7A—O82A—Mo8A—O72A−0.1 (2)Mo3A—O73A—Mo4A—O82A−103.1 (2)
Mo5A—O82A—Mo8A—O72A177.7 (9)Mo8A—O82A—Mo4A—O41A91.0 (7)
Mo7A—O72A—Mo8A—O81A7(3)Mo6A—O82A—Mo4A—O41A−160.5 (8)
Mo1A—O72A—Mo8A—O81A−88 (3)Mo7A—O82A—Mo4A—O41A−14.4 (7)
Mo3A—O72A—Mo8A—O81A101 (3)Mo5A—O82A—Mo4A—O41A−105.2 (6)
Mo2A—O72A—Mo8A—O81A−174 (3)Mo8A—O82A—Mo4A—O42A−77.4 (2)
Mo7A—O72A—Mo8A—O84A−179.7 (2)Mo6A—O82A—Mo4A—O42A31.1 (9)
Mo1A—O72A—Mo8A—O84A85.6 (2)Mo7A—O82A—Mo4A—O42A177.2 (2)
Mo3A—O72A—Mo8A—O84A−85.8 (2)Mo5A—O82A—Mo4A—O42A86.4 (2)
Mo2A—O72A—Mo8A—O84A−0.69 (18)Mo8A—O82A—Mo4A—O43A−177.7 (2)
Mo7A—O72A—Mo8A—O33A−81.0 (2)Mo6A—O82A—Mo4A—O43A−69.2 (9)
Mo1A—O72A—Mo8A—O33A−175.7 (2)Mo7A—O82A—Mo4A—O43A76.9 (2)
Mo3A—O72A—Mo8A—O33A12.98 (18)Mo5A—O82A—Mo4A—O43A−13.91 (16)
Mo2A—O72A—Mo8A—O33A98.06 (19)Mo8A—O82A—Mo4A—O33A17.22 (17)
Mo7A—O72A—Mo8A—O83A81.6 (2)Mo6A—O82A—Mo4A—O33A125.7 (9)
Mo1A—O72A—Mo8A—O83A−13.13 (17)Mo7A—O82A—Mo4A—O33A−88.1 (2)
Mo3A—O72A—Mo8A—O83A175.5 (2)Mo5A—O82A—Mo4A—O33A−179.0 (2)
Mo2A—O72A—Mo8A—O83A−99.39 (19)Mo8A—O82A—Mo4A—O73A93.43 (19)
Mo7A—O72A—Mo8A—O82A0.2 (3)Mo6A—O82A—Mo4A—O73A−158.1 (9)
Mo1A—O72A—Mo8A—O82A−94.56 (19)Mo7A—O82A—Mo4A—O73A−11.92 (15)
Mo3A—O72A—Mo8A—O82A94.09 (18)Mo5A—O82A—Mo4A—O73A−102.75 (18)
Mo2A—O72A—Mo8A—O82A179.17 (13)Mo6A—O53A—Mo5A—O52A−177.1 (3)
Mo5A—O74A—Mo7A—O71A179.5 (3)Mo6A—O53A—Mo5A—O51A−70.8 (3)
Mo5A—O74A—Mo7A—O63A75.8 (3)Mo6A—O53A—Mo5A—O43A45.6 (5)
Mo5A—O74A—Mo7A—O73A−76.8 (3)Mo6A—O53A—Mo5A—O74A92.1 (3)
Mo5A—O74A—Mo7A—O72A−0.5 (7)Mo6A—O53A—Mo5A—O82A20.5 (2)
Mo5A—O74A—Mo7A—O82A−0.8 (2)Mo4A—O43A—Mo5A—O52A177.8 (3)
Mo1A—O63A—Mo7A—O71A75.8 (3)Mo4A—O43A—Mo5A—O51A72.0 (3)
Mo6A—O63A—Mo7A—O71A−170.7 (2)Mo4A—O43A—Mo5A—O53A−44.5 (5)
Mo1A—O63A—Mo7A—O74A−178.4 (2)Mo4A—O43A—Mo5A—O74A−91.0 (3)
Mo6A—O63A—Mo7A—O74A−64.9 (2)Mo4A—O43A—Mo5A—O82A−19.4 (2)
Mo1A—O63A—Mo7A—O73A−62.7 (4)Mo7A—O74A—Mo5A—O52A179.7 (3)
Mo6A—O63A—Mo7A—O73A50.8 (4)Mo7A—O74A—Mo5A—O51A1.2 (9)
Mo1A—O63A—Mo7A—O72A−21.56 (19)Mo7A—O74A—Mo5A—O53A−76.8 (3)
Mo6A—O63A—Mo7A—O72A91.9 (2)Mo7A—O74A—Mo5A—O43A77.9 (3)
Mo1A—O63A—Mo7A—O82A−99.0 (2)Mo7A—O74A—Mo5A—O82A0.8 (2)
Mo6A—O63A—Mo7A—O82A14.46 (19)Mo8A—O82A—Mo5A—O52A177.8 (8)
Mo3A—O73A—Mo7A—O71A−75.2 (3)Mo4A—O82A—Mo5A—O52A92.9 (8)
Mo4A—O73A—Mo7A—O71A170.3 (2)Mo6A—O82A—Mo5A—O52A−100.7 (8)
Mo3A—O73A—Mo7A—O74A179.1 (2)Mo7A—O82A—Mo5A—O52A−4.3 (8)
Mo4A—O73A—Mo7A—O74A64.6 (3)Mo8A—O82A—Mo5A—O51A1.7 (10)
Mo3A—O73A—Mo7A—O63A63.3 (4)Mo4A—O82A—Mo5A—O51A−83.2 (2)
Mo4A—O73A—Mo7A—O63A−51.2 (5)Mo6A—O82A—Mo5A—O51A83.1 (2)
Mo3A—O73A—Mo7A—O72A22.24 (19)Mo7A—O82A—Mo5A—O51A179.6 (2)
Mo4A—O73A—Mo7A—O72A−92.3 (2)Mo8A—O82A—Mo5A—O53A−96.0 (9)
Mo3A—O73A—Mo7A—O82A99.8 (2)Mo4A—O82A—Mo5A—O53A179.2 (2)
Mo4A—O73A—Mo7A—O82A−14.75 (19)Mo6A—O82A—Mo5A—O53A−14.48 (18)
Mo1A—O72A—Mo7A—O71A−82.4 (2)Mo7A—O82A—Mo5A—O53A82.0 (2)
Mo3A—O72A—Mo7A—O71A82.3 (2)Mo8A—O82A—Mo5A—O43A98.8 (10)
Mo8A—O72A—Mo7A—O71A179.5 (2)Mo4A—O82A—Mo5A—O43A13.90 (16)
Mo2A—O72A—Mo7A—O71A3.3 (10)Mo6A—O82A—Mo5A—O43A−179.7 (2)
Mo1A—O72A—Mo7A—O74A97.7 (5)Mo7A—O82A—Mo5A—O43A−83.29 (19)
Mo3A—O72A—Mo7A—O74A−97.7 (5)Mo8A—O82A—Mo5A—O74A−178.5 (10)
Mo8A—O72A—Mo7A—O74A−0.4 (6)Mo4A—O82A—Mo5A—O74A96.67 (19)
Mo2A—O72A—Mo7A—O74A−176.6 (7)Mo6A—O82A—Mo5A—O74A−96.98 (18)
Mo1A—O72A—Mo7A—O63A17.57 (16)Mo7A—O82A—Mo5A—O74A−0.52 (16)
Mo3A—O72A—Mo7A—O63A−177.78 (19)Mo5B—O43B—Mo4B—O41B180.0 (3)
Mo8A—O72A—Mo7A—O63A−80.5 (2)Mo5B—O43B—Mo4B—O42B−71.7 (3)
Mo2A—O72A—Mo7A—O63A103.2 (9)Mo5B—O43B—Mo4B—O33B49.2 (5)
Mo1A—O72A—Mo7A—O73A177.70 (19)Mo5B—O43B—Mo4B—O73B92.7 (3)
Mo3A—O72A—Mo7A—O73A−17.64 (15)Mo5B—O43B—Mo4B—O82B20.7 (2)
Mo8A—O72A—Mo7A—O73A79.60 (19)Mo8B—O33B—Mo4B—O41B179.5 (3)
Mo2A—O72A—Mo7A—O73A−96.6 (10)Mo3B—O33B—Mo4B—O41B−62.4 (2)
Mo1A—O72A—Mo7A—O82A97.96 (16)Mo8B—O33B—Mo4B—O42B72.9 (3)
Mo3A—O72A—Mo7A—O82A−97.39 (15)Mo3B—O33B—Mo4B—O42B−169.1 (2)
Mo8A—O72A—Mo7A—O82A−0.1 (2)Mo8B—O33B—Mo4B—O43B−49.5 (4)
Mo2A—O72A—Mo7A—O82A−176.4 (9)Mo3B—O33B—Mo4B—O43B68.5 (4)
Mo8A—O82A—Mo7A—O71A−4(3)Mo8B—O33B—Mo4B—O73B−95.6 (2)
Mo4A—O82A—Mo7A—O71A91 (3)Mo3B—O33B—Mo4B—O73B22.40 (16)
Mo6A—O82A—Mo7A—O71A−98 (3)Mo8B—O33B—Mo4B—O82B−20.18 (19)
Mo5A—O82A—Mo7A—O71A177 (3)Mo3B—O33B—Mo4B—O82B97.8 (2)
Mo8A—O82A—Mo7A—O74A−180.0 (3)Mo7B—O73B—Mo4B—O41B−166.5 (3)
Mo4A—O82A—Mo7A—O74A−85.1 (2)Mo3B—O73B—Mo4B—O41B75.5 (2)
Mo6A—O82A—Mo7A—O74A85.6 (2)Mo7B—O73B—Mo4B—O42B47.1 (8)
Mo5A—O82A—Mo7A—O74A0.6 (2)Mo3B—O73B—Mo4B—O42B−70.9 (8)
Mo8A—O82A—Mo7A—O63A81.1 (2)Mo7B—O73B—Mo4B—O43B−64.7 (3)
Mo4A—O82A—Mo7A—O63A175.9 (2)Mo3B—O73B—Mo4B—O43B177.3 (2)
Mo6A—O82A—Mo7A—O63A−13.35 (18)Mo7B—O73B—Mo4B—O33B91.6 (2)
Mo5A—O82A—Mo7A—O63A−98.34 (19)Mo3B—O73B—Mo4B—O33B−26.4 (2)
Mo8A—O82A—Mo7A—O73A−81.0 (2)Mo7B—O73B—Mo4B—O82B14.5 (2)
Mo4A—O82A—Mo7A—O73A13.81 (17)Mo3B—O73B—Mo4B—O82B−103.5 (2)
Mo6A—O82A—Mo7A—O73A−175.4 (2)Mo8B—O82B—Mo4B—O41B91.1 (6)
Mo5A—O82A—Mo7A—O73A99.6 (2)Mo7B—O82B—Mo4B—O41B−14.0 (7)
Mo8A—O82A—Mo7A—O72A0.2 (3)Mo6B—O82B—Mo4B—O41B−161.4 (7)
Mo4A—O82A—Mo7A—O72A94.97 (19)Mo5B—O82B—Mo4B—O41B−104.7 (6)
Mo6A—O82A—Mo7A—O72A−94.26 (17)Mo8B—O82B—Mo4B—O42B−77.4 (2)
Mo5A—O82A—Mo7A—O72A−179.25 (13)Mo7B—O82B—Mo4B—O42B177.5 (2)
Mo5B—O74B—Mo7B—O71B−179.8 (3)Mo6B—O82B—Mo4B—O42B30.2 (9)
Mo5B—O74B—Mo7B—O63B76.0 (3)Mo5B—O82B—Mo4B—O42B86.8 (2)
Mo5B—O74B—Mo7B—O73B−77.3 (3)Mo8B—O82B—Mo4B—O43B−178.6 (2)
Mo5B—O74B—Mo7B—O72B−0.1 (7)Mo7B—O82B—Mo4B—O43B76.3 (2)
Mo5B—O74B—Mo7B—O82B−0.8 (2)Mo6B—O82B—Mo4B—O43B−71.0 (8)
Mo1B—O63B—Mo7B—O71B75.3 (3)Mo5B—O82B—Mo4B—O43B−14.36 (16)
Mo6B—O63B—Mo7B—O71B−170.5 (2)Mo8B—O82B—Mo4B—O33B17.57 (17)
Mo1B—O63B—Mo7B—O74B−179.5 (2)Mo7B—O82B—Mo4B—O33B−87.5 (2)
Mo6B—O63B—Mo7B—O74B−65.3 (2)Mo6B—O82B—Mo4B—O33B125.1 (9)
Mo1B—O63B—Mo7B—O73B−65.0 (4)Mo5B—O82B—Mo4B—O33B−178.2 (2)
Mo6B—O63B—Mo7B—O73B49.2 (5)Mo8B—O82B—Mo4B—O73B93.79 (19)
Mo1B—O63B—Mo7B—O72B−22.4 (2)Mo7B—O82B—Mo4B—O73B−11.32 (15)
Mo6B—O63B—Mo7B—O72B91.8 (2)Mo6B—O82B—Mo4B—O73B−158.7 (9)
Mo1B—O63B—Mo7B—O82B−100.2 (2)Mo5B—O82B—Mo4B—O73B−102.02 (17)
Mo6B—O63B—Mo7B—O82B14.1 (2)Mo2A—O13A—Mo1A—O11A180.0 (3)
Mo3B—O73B—Mo7B—O71B−76.1 (3)Mo2A—O13A—Mo1A—O12A72.9 (3)
Mo4B—O73B—Mo7B—O71B170.3 (2)Mo2A—O13A—Mo1A—O63A−47.6 (5)
Mo3B—O73B—Mo7B—O74B178.9 (2)Mo2A—O13A—Mo1A—O83A−92.2 (3)
Mo4B—O73B—Mo7B—O74B65.3 (2)Mo2A—O13A—Mo1A—O72A−19.5 (2)
Mo3B—O73B—Mo7B—O63B64.5 (4)Mo7A—O63A—Mo1A—O11A−178.2 (2)
Mo4B—O73B—Mo7B—O63B−49.1 (5)Mo6A—O63A—Mo1A—O11A63.6 (2)
Mo3B—O73B—Mo7B—O72B21.96 (19)Mo7A—O63A—Mo1A—O12A−72.5 (3)
Mo4B—O73B—Mo7B—O72B−91.7 (2)Mo6A—O63A—Mo1A—O12A169.3 (2)
Mo3B—O73B—Mo7B—O82B99.7 (2)Mo7A—O63A—Mo1A—O13A49.1 (4)
Mo4B—O73B—Mo7B—O82B−13.94 (19)Mo6A—O63A—Mo1A—O13A−69.1 (4)
Mo1B—O72B—Mo7B—O71B−82.6 (2)Mo7A—O63A—Mo1A—O83A96.5 (2)
Mo8B—O72B—Mo7B—O71B179.2 (2)Mo6A—O63A—Mo1A—O83A−21.72 (17)
Mo3B—O72B—Mo7B—O71B82.0 (2)Mo7A—O63A—Mo1A—O72A20.40 (18)
Mo2B—O72B—Mo7B—O71B2.5 (10)Mo6A—O63A—Mo1A—O72A−97.8 (2)
Mo1B—O72B—Mo7B—O74B97.7 (5)Mo8A—O83A—Mo1A—O11A166.2 (3)
Mo8B—O72B—Mo7B—O74B−0.6 (6)Mo6A—O83A—Mo1A—O11A−76.4 (2)
Mo3B—O72B—Mo7B—O74B−97.7 (5)Mo8A—O83A—Mo1A—O12A−48.8 (9)
Mo2B—O72B—Mo7B—O74B−177.2 (7)Mo6A—O83A—Mo1A—O12A68.6 (8)
Mo1B—O72B—Mo7B—O63B17.98 (16)Mo8A—O83A—Mo1A—O13A64.2 (2)
Mo8B—O72B—Mo7B—O63B−80.2 (2)Mo6A—O83A—Mo1A—O13A−178.4 (2)
Mo3B—O72B—Mo7B—O63B−177.39 (19)Mo8A—O83A—Mo1A—O63A−92.2 (3)
Mo2B—O72B—Mo7B—O63B103.1 (10)Mo6A—O83A—Mo1A—O63A25.15 (19)
Mo1B—O72B—Mo7B—O73B178.23 (19)Mo8A—O83A—Mo1A—O72A−14.6 (2)
Mo8B—O72B—Mo7B—O73B80.02 (19)Mo6A—O83A—Mo1A—O72A102.7 (2)
Mo3B—O72B—Mo7B—O73B−17.14 (15)Mo7A—O72A—Mo1A—O11A−90.8 (7)
Mo2B—O72B—Mo7B—O73B−96.7 (10)Mo3A—O72A—Mo1A—O11A161.3 (7)
Mo1B—O72B—Mo7B—O82B98.32 (15)Mo8A—O72A—Mo1A—O11A13.8 (7)
Mo8B—O72B—Mo7B—O82B0.1 (2)Mo2A—O72A—Mo1A—O11A104.4 (6)
Mo3B—O72B—Mo7B—O82B−97.05 (15)Mo7A—O72A—Mo1A—O12A77.8 (2)
Mo2B—O72B—Mo7B—O82B−176.6 (9)Mo3A—O72A—Mo1A—O12A−30.1 (9)
Mo8B—O82B—Mo7B—O71B−12 (3)Mo8A—O72A—Mo1A—O12A−177.6 (2)
Mo4B—O82B—Mo7B—O71B83 (3)Mo2A—O72A—Mo1A—O12A−87.0 (2)
Mo6B—O82B—Mo7B—O71B−106 (3)Mo7A—O72A—Mo1A—O13A178.1 (2)
Mo5B—O82B—Mo7B—O71B169 (3)Mo3A—O72A—Mo1A—O13A70.1 (9)
Mo8B—O82B—Mo7B—O74B179.6 (3)Mo8A—O72A—Mo1A—O13A−77.3 (2)
Mo4B—O82B—Mo7B—O74B−85.3 (2)Mo2A—O72A—Mo1A—O13A13.19 (16)
Mo6B—O82B—Mo7B—O74B85.6 (2)Mo7A—O72A—Mo1A—O63A−17.38 (16)
Mo5B—O82B—Mo7B—O74B0.65 (19)Mo3A—O72A—Mo1A—O63A−125.3 (9)
Mo8B—O82B—Mo7B—O63B81.2 (2)Mo8A—O72A—Mo1A—O63A87.23 (19)
Mo4B—O82B—Mo7B—O63B176.3 (2)Mo2A—O72A—Mo1A—O63A177.75 (18)
Mo6B—O82B—Mo7B—O63B−12.77 (18)Mo7A—O72A—Mo1A—O83A−93.26 (18)
Mo5B—O82B—Mo7B—O63B−97.7 (2)Mo3A—O72A—Mo1A—O83A158.8 (9)
Mo8B—O82B—Mo7B—O73B−82.0 (2)Mo8A—O72A—Mo1A—O83A11.36 (15)
Mo4B—O82B—Mo7B—O73B13.08 (17)Mo2A—O72A—Mo1A—O83A101.88 (17)
Mo6B—O82B—Mo7B—O73B−176.0 (2)Mo2B—O13B—Mo1B—O11B179.4 (3)
Mo5B—O82B—Mo7B—O73B99.08 (19)Mo2B—O13B—Mo1B—O12B72.1 (3)
Mo8B—O82B—Mo7B—O72B−0.1 (3)Mo2B—O13B—Mo1B—O63B−48.8 (5)
Mo4B—O82B—Mo7B—O72B94.92 (19)Mo2B—O13B—Mo1B—O72B−20.0 (2)
Mo6B—O82B—Mo7B—O72B−94.13 (17)Mo2B—O13B—Mo1B—O83B−92.5 (3)
Mo5B—O82B—Mo7B—O72B−179.08 (13)Mo7B—O63B—Mo1B—O11B−177.9 (2)
Mo6B—O53B—Mo5B—O52B−177.4 (3)Mo6B—O63B—Mo1B—O11B62.8 (2)
Mo6B—O53B—Mo5B—O51B−70.0 (3)Mo7B—O63B—Mo1B—O12B−72.0 (3)
Mo6B—O53B—Mo5B—O43B45.1 (5)Mo6B—O63B—Mo1B—O12B168.7 (2)
Mo6B—O53B—Mo5B—O74B92.4 (3)Mo7B—O63B—Mo1B—O13B50.3 (4)
Mo6B—O53B—Mo5B—O82B20.2 (3)Mo6B—O63B—Mo1B—O13B−69.1 (4)
Mo4B—O43B—Mo5B—O52B177.0 (3)Mo7B—O63B—Mo1B—O72B20.86 (19)
Mo4B—O43B—Mo5B—O51B70.1 (3)Mo6B—O63B—Mo1B—O72B−98.5 (2)
Mo4B—O43B—Mo5B—O53B−45.0 (5)Mo7B—O63B—Mo1B—O83B96.9 (2)
Mo4B—O43B—Mo5B—O74B−92.5 (3)Mo6B—O63B—Mo1B—O83B−22.47 (16)
Mo4B—O43B—Mo5B—O82B−20.0 (2)Mo7B—O72B—Mo1B—O11B−92.9 (7)
Mo7B—O74B—Mo5B—O52B179.0 (3)Mo8B—O72B—Mo1B—O11B11.2 (7)
Mo7B—O74B—Mo5B—O51B1.9 (9)Mo3B—O72B—Mo1B—O11B161.8 (8)
Mo7B—O74B—Mo5B—O53B−77.2 (3)Mo2B—O72B—Mo1B—O11B102.6 (6)
Mo7B—O74B—Mo5B—O43B77.9 (3)Mo7B—O72B—Mo1B—O12B77.6 (2)
Mo7B—O74B—Mo5B—O82B0.8 (2)Mo8B—O72B—Mo1B—O12B−178.3 (2)
Mo8B—O82B—Mo5B—O52B177.1 (8)Mo3B—O72B—Mo1B—O12B−27.7 (9)
Mo4B—O82B—Mo5B—O52B90.8 (7)Mo2B—O72B—Mo1B—O12B−86.9 (2)
Mo7B—O82B—Mo5B—O52B−6.7 (8)Mo7B—O72B—Mo1B—O13B178.6 (2)
Mo6B—O82B—Mo5B—O52B−103.2 (7)Mo8B—O72B—Mo1B—O13B−77.4 (2)
Mo8B—O82B—Mo5B—O51B3.5 (10)Mo3B—O72B—Mo1B—O13B73.3 (8)
Mo4B—O82B—Mo5B—O51B−82.7 (2)Mo2B—O72B—Mo1B—O13B14.04 (16)
Mo7B—O82B—Mo5B—O51B179.8 (2)Mo7B—O72B—Mo1B—O63B−17.91 (16)
Mo6B—O82B—Mo5B—O51B83.2 (2)Mo8B—O72B—Mo1B—O63B86.15 (19)
Mo8B—O82B—Mo5B—O53B−93.8 (10)Mo3B—O72B—Mo1B—O63B−123.2 (9)
Mo4B—O82B—Mo5B—O53B180.0 (2)Mo2B—O72B—Mo1B—O63B177.56 (19)
Mo7B—O82B—Mo5B—O53B82.5 (2)Mo7B—O72B—Mo1B—O83B−93.17 (19)
Mo6B—O82B—Mo5B—O53B−14.07 (19)Mo8B—O72B—Mo1B—O83B10.88 (15)
Mo8B—O82B—Mo5B—O43B100.4 (10)Mo3B—O72B—Mo1B—O83B161.6 (9)
Mo4B—O82B—Mo5B—O43B14.18 (16)Mo2B—O72B—Mo1B—O83B102.30 (17)
Mo7B—O82B—Mo5B—O43B−83.29 (19)Mo8B—O83B—Mo1B—O11B166.2 (3)
Mo6B—O82B—Mo5B—O43B−179.9 (2)Mo6B—O83B—Mo1B—O11B−76.1 (3)
Mo8B—O82B—Mo5B—O74B−176.8 (10)Mo8B—O83B—Mo1B—O12B−48.4 (9)
Mo4B—O82B—Mo5B—O74B96.93 (18)Mo6B—O83B—Mo1B—O12B69.3 (8)
Mo7B—O82B—Mo5B—O74B−0.54 (16)Mo8B—O83B—Mo1B—O13B64.4 (3)
Mo6B—O82B—Mo5B—O74B−97.12 (18)Mo6B—O83B—Mo1B—O13B−178.0 (2)
Mo2A—O23A—Mo3A—O31A−177.3 (3)Mo8B—O83B—Mo1B—O63B−91.3 (3)
Mo2A—O23A—Mo3A—O32A−69.9 (3)Mo6B—O83B—Mo1B—O63B26.34 (19)
Mo2A—O23A—Mo3A—O73A50.9 (5)Mo8B—O83B—Mo1B—O72B−13.9 (2)
Mo2A—O23A—Mo3A—O33A93.9 (3)Mo6B—O83B—Mo1B—O72B103.8 (2)
Mo2A—O23A—Mo3A—O72A21.1 (2)C18B—C17B—N1B—C15B56.3 (13)
Mo7A—O73A—Mo3A—O31A176.3 (3)C18B—C17B—N1B—C11B177.0 (11)
Mo4A—O73A—Mo3A—O31A−64.9 (3)C18B—C17B—N1B—C13B−62.3 (13)
Mo7A—O73A—Mo3A—O32A70.2 (3)C16B—C15B—N1B—C17B51.9 (13)
Mo4A—O73A—Mo3A—O32A−171.0 (2)C16B—C15B—N1B—C11B−64.8 (12)
Mo7A—O73A—Mo3A—O23A−51.4 (4)C16B—C15B—N1B—C13B173.5 (10)
Mo4A—O73A—Mo3A—O23A67.4 (4)C12B—C11B—N1B—C17B174.3 (10)
Mo7A—O73A—Mo3A—O33A−97.0 (2)C12B—C11B—N1B—C15B−65.1 (12)
Mo4A—O73A—Mo3A—O33A21.82 (17)C12B—C11B—N1B—C13B53.6 (13)
Mo7A—O73A—Mo3A—O72A−20.76 (18)C14B—C13B—N1B—C17B−59.8 (11)
Mo4A—O73A—Mo3A—O72A98.0 (2)C14B—C13B—N1B—C15B178.6 (9)
Mo8A—O33A—Mo3A—O31A−167.5 (3)C14B—C13B—N1B—C11B56.9 (11)
Mo4A—O33A—Mo3A—O31A75.9 (2)C36A—C35A—N3A—C37A−50.5 (12)
Mo8A—O33A—Mo3A—O32A41.6 (9)C36A—C35A—N3A—C33A−171.7 (9)
Mo4A—O33A—Mo3A—O32A−75.0 (8)C36A—C35A—N3A—C31A67.8 (11)
Mo8A—O33A—Mo3A—O23A−64.9 (2)C38A—C37A—N3A—C35A−58.9 (10)
Mo4A—O33A—Mo3A—O23A178.5 (2)C38A—C37A—N3A—C33A58.6 (10)
Mo8A—O33A—Mo3A—O73A91.4 (3)C38A—C37A—N3A—C31A−179.5 (9)
Mo4A—O33A—Mo3A—O73A−25.2 (2)C34A—C33A—N3A—C35A−177.7 (10)
Mo8A—O33A—Mo3A—O72A14.4 (2)C34A—C33A—N3A—C37A60.4 (12)
Mo4A—O33A—Mo3A—O72A−102.2 (2)C34A—C33A—N3A—C31A−58.3 (12)
Mo7A—O72A—Mo3A—O31A87.3 (7)C32A—C31A—N3A—C35A58.3 (12)
Mo1A—O72A—Mo3A—O31A−164.7 (8)C32A—C31A—N3A—C37A−179.6 (9)
Mo8A—O72A—Mo3A—O31A−17.2 (8)C32A—C31A—N3A—C33A−58.0 (12)
Mo2A—O72A—Mo3A—O31A−107.6 (7)C38B—C37B—N3B—C33B60.3 (12)
Mo7A—O72A—Mo3A—O32A−79.1 (2)C38B—C37B—N3B—C35B−58.5 (12)
Mo1A—O72A—Mo3A—O32A28.9 (9)C38B—C37B—N3B—C31B−177.6 (9)
Mo8A—O72A—Mo3A—O32A176.4 (2)C34B—C33B—N3B—C37B61.5 (14)
Mo2A—O72A—Mo3A—O32A86.0 (2)C34B—C33B—N3B—C35B−176.6 (12)
Mo7A—O72A—Mo3A—O23A−179.4 (2)C34B—C33B—N3B—C31B−55.0 (15)
Mo1A—O72A—Mo3A—O23A−71.4 (9)C36B—C35B—N3B—C37B−50.2 (16)
Mo8A—O72A—Mo3A—O23A76.1 (2)C36B—C35B—N3B—C33B−171.4 (12)
Mo2A—O72A—Mo3A—O23A−14.33 (17)C36B—C35B—N3B—C31B65.1 (15)
Mo7A—O72A—Mo3A—O73A17.58 (16)C32B—C31B—N3B—C37B−174.9 (11)
Mo1A—O72A—Mo3A—O73A125.6 (9)C32B—C31B—N3B—C33B−54.6 (15)
Mo8A—O72A—Mo3A—O73A−86.90 (18)C32B—C31B—N3B—C35B64.9 (13)
Mo2A—O72A—Mo3A—O73A−177.34 (19)C22B—C21B—N2B—C27B57.7 (12)
Mo7A—O72A—Mo3A—O33A93.35 (18)C22B—C21B—N2B—C23B−179.5 (9)
Mo1A—O72A—Mo3A—O33A−158.6 (9)C22B—C21B—N2B—C25B−61.1 (11)
Mo8A—O72A—Mo3A—O33A−11.13 (16)C28B—C27B—N2B—C21B57.7 (12)
Mo2A—O72A—Mo3A—O33A−101.57 (17)C28B—C27B—N2B—C23B−61.8 (11)
Mo2B—O23B—Mo3B—O31B−178.8 (3)C28B—C27B—N2B—C25B178.1 (10)
Mo2B—O23B—Mo3B—O32B−70.6 (3)C24B—C23B—N2B—C21B178.0 (9)
Mo2B—O23B—Mo3B—O73B47.8 (5)C24B—C23B—N2B—C27B−58.4 (11)
Mo2B—O23B—Mo3B—O33B92.7 (3)C24B—C23B—N2B—C25B59.8 (11)
Mo2B—O23B—Mo3B—O72B20.5 (2)C26B—C25B—N2B—C21B−59.6 (11)
Mo7B—O73B—Mo3B—O31B178.1 (2)C26B—C25B—N2B—C27B177.6 (9)
Mo4B—O73B—Mo3B—O31B−63.7 (2)C26B—C25B—N2B—C23B56.3 (10)
Mo7B—O73B—Mo3B—O32B71.5 (3)C28A—C27A—N2A—C21A−58.0 (10)
Mo4B—O73B—Mo3B—O32B−170.4 (2)C28A—C27A—N2A—C23A59.8 (10)
Mo7B—O73B—Mo3B—O23B−48.0 (4)C28A—C27A—N2A—C25A−179.5 (9)
Mo4B—O73B—Mo3B—O23B70.1 (4)C22A—C21A—N2A—C27A−56.8 (11)
Mo7B—O73B—Mo3B—O33B−95.7 (2)C22A—C21A—N2A—C23A−177.4 (9)
Mo4B—O73B—Mo3B—O33B22.49 (17)C22A—C21A—N2A—C25A61.9 (11)
Mo7B—O73B—Mo3B—O72B−20.11 (18)C24A—C23A—N2A—C27A57.0 (11)
Mo4B—O73B—Mo3B—O72B98.1 (2)C24A—C23A—N2A—C21A179.1 (9)
Mo8B—O33B—Mo3B—O31B−167.8 (3)C24A—C23A—N2A—C25A−60.5 (11)
Mo4B—O33B—Mo3B—O31B75.4 (2)C26A—C25A—N2A—C27A177.8 (10)
Mo8B—O33B—Mo3B—O32B41.5 (9)C26A—C25A—N2A—C21A55.0 (12)
Mo4B—O33B—Mo3B—O32B−75.3 (8)C26A—C25A—N2A—C23A−62.1 (12)
Mo8B—O33B—Mo3B—O23B−64.1 (2)C18A—C17A—N1A—C15A56.4 (16)
Mo4B—O33B—Mo3B—O23B179.0 (2)C18A—C17A—N1A—C13A−62.4 (16)
Mo8B—O33B—Mo3B—O73B90.5 (2)C18A—C17A—N1A—C11A176.3 (13)
Mo4B—O33B—Mo3B—O73B−26.3 (2)C16A—C15A—N1A—C17A52.0 (16)
Mo8B—O33B—Mo3B—O72B13.6 (2)C16A—C15A—N1A—C13A176.7 (12)
Mo4B—O33B—Mo3B—O72B−103.2 (2)C16A—C15A—N1A—C11A−63.7 (14)
Mo7B—O72B—Mo3B—O31B88.9 (7)C14A—C13A—N1A—C17A−59.1 (14)
Mo1B—O72B—Mo3B—O31B−165.8 (8)C14A—C13A—N1A—C15A178.6 (10)
Mo8B—O72B—Mo3B—O31B−15.0 (7)C14A—C13A—N1A—C11A58.6 (12)
Mo2B—O72B—Mo3B—O31B−106.4 (6)C12A—C11A—N1A—C17A−179.2 (12)
Mo7B—O72B—Mo3B—O32B−78.8 (2)C12A—C11A—N1A—C15A−59.4 (14)
Mo1B—O72B—Mo3B—O32B26.6 (9)C12A—C11A—N1A—C13A56.7 (15)

Hydrogen-bond geometry (Å, °)

D—H···AD—HH···AD···AD—H···A
N4A—H1N···O12B0.822.399 (6)2.908 (10)121.32 (58)
N4A—H1N···O21B0.822.388 (5)2.851 (10)116.76 (59)
N4A—H1N···O32B0.822.571 (5)2.936 (9)108.68 (57)
N4A—H1N···O71B0.822.482 (5)2.904 (10)113.29 (55)
N4A—H2N···O42A0.962.457 (5)2.856 (10)104.87 (51)
N4A—H2N···O51A0.962.216 (5)2.915 (10)129.21 (53)
N4A—H3N···O12B0.732.566 (6)2.908 (10)110.92 (67)
N4A—H3N···O62A0.732.261 (5)2.909 (9)148.30 (5)
N4A—H4N···O42A0.962.511 (6)2.856 (10)101.14 (51)
N4A—H4N···O81A0.961.999 (5)2.865 (10)149.24 (50)
N4B—H5N···O12Ai0.842.441 (6)2.854 (10)110.89 (56)
N4B—H5N···O32Ai0.842.445 (5)2.950 (9)119.12 (54)
N4B—H5N···O71Ai0.842.458 (6)2.943 (10)117.38 (53)
N4B—H6N···O12Ai0.952.387 (5)2.854 (10)109.94 (50)
N4B—H6N···O62B0.952.214 (5)2.992 (9)138.49 (51)
N4B—H7N···O42B0.972.385 (6)2.820 (10)106.78 (50)
N4B—H7N···O81B0.972.089 (5)2.895 (10)139.63 (48)
N4B—H8N···O51B0.962.122 (5)2.855 (10)132.53 (52)

Symmetry codes: (i) x, y, z−1.

Footnotes

Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: BT2676).

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