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Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.043Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.117H-atom parameters constrained
S = 1.06w = 1/[σ2(Fo2) + (0.0469P)2 + 1.2301P] where P = (Fo2 + 2Fc2)/3
2750 reflections(Δ/σ)max < 0.001
155 parametersΔρmax = 0.20 e Å3
0 restraintsΔρmin = −0.25 e Å3